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| Content Provider | IEEE Xplore Digital Library |
|---|---|
| Author | Rongfeng Guan Wenqing Zhao Shuaimou Li |
| Copyright Year | 2009 |
| Description | Author affiliation: Institute of Materials Science and Engineering, Henan Polytechnic University No. 2001, Century Avenue, Jiaozuo 454003, Henan Province, China (Rongfeng Guan; Wenqing Zhao; Shuaimou Li) |
| Abstract | In recent years, the preparation technology of the white light LED packaged YAG phosphor develops very quickly. The preparation methods include solid-phase method, sol-gel method, precipitation method, combustion method and so on. The traditional solid-phase method is still dominant in all of them, whereas this method also has shortcomings such as a high synthesis temperature, longer reaction time, bulky grains and larger hardness. So it requires a new approach to achieve the phosphor synthesis. Using metal nitrate as raw materials and citric acid as a complexing agent, we prepared $Y3A15O12:Ce^{3+}$ yellow phosphor by the sol-gel method (sol-gel). The X-ray powder diffraction (XRD) shows that it has been pure yttrium aluminum garnet phase (YAG) at 900°C. The infrared absorption spectra of the powders show that YAG phase has been formed when the calcination temperature is 900°C, because there are the characteristic vibrational peaks of metal and oxygen atoms, which are in the low-frequency area at $724cm^{−1},$ $792cm^{−1}$ peak. With scanning electron microscopy (SEM) analysis of its morphology, the result proves the grain diameter ranges from 1 to 3μm, averaged at 2μm. Their fluorescence spectra were studied using fluorescence spectrometer and the results show luminous intensity reach at the maximum when calcination temperature up to 1200°C. |
| Starting Page | 786 |
| Ending Page | 789 |
| File Size | 778000 |
| Page Count | 4 |
| File Format | |
| ISBN | 9781424446582 |
| DOI | 10.1109/ICEPT.2009.5270641 |
| Language | English |
| Publisher | Institute of Electrical and Electronics Engineers, Inc. (IEEE) |
| Publisher Date | 2009-08-10 |
| Publisher Place | China |
| Access Restriction | Subscribed |
| Rights Holder | Institute of Electrical and Electronics Engineers, Inc. (IEEE) |
| Subject Keyword | Light emitting diodes Packaging Phosphors Temperature Powders Calcination Scanning electron microscopy Fluorescence Combustion Raw materials |
| Content Type | Text |
| Resource Type | Article |
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