NDLI: High-Resolution Trace Element Profiles in Calcium Carbonate Shells using LA-ICP-MS: An Environmental Proxy and Biogeochemical Cycling?

Content Provider	IEEE Xplore Digital Library
Author	Wei Guo Shenghong Hu Yuee Peng
Copyright Year	2008
Description	Author affiliation: Fac. of Earth Sci. China, Univ. of Geosci. Wuhan, Wuhan (Wei Guo; Shenghong Hu)
Abstract	In this study we have used 193 ArF excimer laser ablation inductively coupled plasma mass spectrometry (LA-ICP-MS), to produce a high resolution (32 mum) shells record of Mn, Zn, Sr, Ba, Mg, Cr, Cu, As, Cd, Co and Pb for the Periglypta reticulate and Tridacna gigas mussel shells from the Yalong bay, Hainan Island of China. Our synthesized $CaCO_{3}$ co-precipitation multi-elements discs as the solid matrix- matched standards for calibration, and 42 bCa was selected as the internal standard to compensate the draft of signal. The results also demonstrated our co-precipitation matrix matched calibration method was more appropriate than the commercial NIST610/612 glass standards calibration method. Validation of the matrix- matched LA- ICP-MS technique indicated that the method provides accurate and reproducible (RSD<10%) analysis of trace elements in shells (0.01~3000 mug/g). The detection limits of this method for these elements were obtained in the range of 0.103 to 0.709 mug /g with correlation coefficients (R) better than 0.993. The proposed method was successfully applied to determine the trace elements in the two shells. The high-resolution trace element profiles could be as an environmental proxy and biogeochemical cycling for the area in which the fish or mussel lives.
Starting Page	4480
Ending Page	4483
File Size	460535
Page Count	4
File Format	PDF
ISBN	9781424417476
DOI	10.1109/ICBBE.2008.613
Language	English
Publisher	Institute of Electrical and Electronics Engineers, Inc. (IEEE)
Publisher Date	2008-05-16
Publisher Place	China
Access Restriction	Subscribed
Rights Holder	Institute of Electrical and Electronics Engineers, Inc. (IEEE)
Subject Keyword	Strontium Calcium Chromium Mass spectroscopy Optical coupling Calibration Laser ablation Plasmas Signal synthesis Zinc
Content Type	Text
Resource Type	Article

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