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| Content Provider | World Health Organization (WHO)-Global Index Medicus |
|---|---|
| Author | Tang, Huaqi Zhang, Xinyue Luo, Shilin Shang, Fei Chen, Jianping Wang, Jinghong Duan, Xiaojie Gao, Xiaoyan Sun, Yikun |
| Description | Country affiliation: China Author Affiliation: Tang H ( a School of Chinese Materia Medica , Beijing University of Chinese Medicine , Beijing , China.); Zhang X ( a School of Chinese Materia Medica , Beijing University of Chinese Medicine , Beijing , China.); Luo S ( a School of Chinese Materia Medica , Beijing University of Chinese Medicine , Beijing , China.); Shang F ( b Analytical and Testing Center , Beijing University of Chemical Technology , Beijing , China.); Chen J ( c College of Pharmacy , Inner Mongolia Medical University , Hohhot , China.); Wang J ( d Pharmacy Department , Wangjing Hospital of China Academy of Chinese Medical Sciences , Beijing , China.); Duan X ( a School of Chinese Materia Medica , Beijing University of Chinese Medicine , Beijing , China.); Gao X ( a School of Chinese Materia Medica , Beijing University of Chinese Medicine , Beijing , China.); Sun Y ( a School of Chinese Materia Medica , Beijing University of Chinese Medicine , Beijing , China.) |
| Abstract | Xuan Hu Suo San (XHSS) is a traditional Chinese medicine that has been extensively applied in the treatment of osteoarthritis for many years, however, its chemical composition has not yet been elucidated. Thus, a rapid, efficient, and precise method based on ultra high performance liquid chromatography coupled with quadrupole time-of-flight mass spectrometry was applied in both positive- and negative-ion modes to rapidly separate and identify the main chemical ingredients in XHSS for the first time. Finally, with the optimised separation and detection method, a total of 57 compounds were simultaneously separated within 13 min, among which 14 compounds were confirmed by comparing retention time and MS data with reference standards and others were tentatively identified by comparing with reference literatures. This rapid and sensitive approach is highly useful for the identification and characterisation of chemical constituents, and provides fundamental and extensive information supporting further metabolic and pharmacokinetic studies of XHSS. |
| File Format | HTM / HTML |
| ISSN | 14786419 |
| Journal | Natural Product Research |
| e-ISSN | 14786427 |
| Language | English |
| Publisher | Taylor & Francis |
| Publisher Date | 2017-02-15 |
| Publisher Place | Great Britain (UK) |
| Access Restriction | One Nation One Subscription (ONOS) |
| Subject Keyword | Discipline Natural Products |
| Content Type | Text |
| Resource Type | Article |
| Subject | Organic Chemistry Plant Science Analytical Chemistry Biochemistry |
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