NDLI: Crystal structure, spectral, thermal and dielectric studies of a new zinc benzoate single crystal.

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Crystal structure, spectral, thermal and dielectric studies of a new zinc benzoate single crystal.

Content Provider	World Health Organization (WHO)-Global Index Medicus
Author	Nair, C. M. K. Deepa, M. Bijini, B. R. Prasanna, S. Rajendra Babu, K.
Description	Country affiliation: India Author Affiliation: Bijini BR ( Deparetment of Physics, M.G. College, Thiruvananthapuram 695004, India.)
Abstract	Single crystals of zinc benzoate with a novel structure were grown in gel media. Sodium metasilicate of gel density 1.04 g/cc at pH 6 was employed to yield transparent single crystals. The crystal structure of the compound was ascertained by single crystal X-ray diffractometry. It was noted that the crystal belongs to monoclinic system with space group P2(1)/c with unit cell parameters a=10.669(1)Å, b=12.995(5)Å, c=19.119(3)Å, and ß=94.926(3)°. The crystal was seen to possess a linear polymeric structure along b-axis; with no presence of coordinated or lattice water. CHN analysis established the stoichiometric composition of the crystal. The existence of functional groups present in the single crystal system was confirmed by FT-IR studies. The thermal characteristic of the sample was analysed by TGA-DTA techniques, and the sample was found to be thermally stable up to 280°C. The kinetic and thermodynamic parameters were also determined. UV-Vis spectroscopy corroborated the transparency of the crystal and revealed the optical band gap to be 4 eV. Dielectric studies showed decrease in the dielectric constant of the sample with increase in frequency.
ISSN	13861425
Volume Number	97
e-ISSN	18733557
Journal	Spectrochimica Acta Part A: Molecular and Biomolecular Spectroscopy
Language	English
Publisher	Elsevier
Publisher Date	2012-11-01
Publisher Place	Great Britain (UK)
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	Dielectric Spectroscopy Temperature Zinc Compounds Chemistry Zinc Crystallization Crystallography, X-ray Kinetics Molecular Conformation Spectrophotometry, Ultraviolet Spectroscopy, Fourier Transform Infrared Spectroscopy, Near-infrared Torsion, Mechanical Journal Article Discipline Spectroscopy
Content Type	Text
Resource Type	Article
Subject	Spectroscopy Atomic and Molecular Physics, and Optics Analytical Chemistry Instrumentation

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