NDLI: Synthesis and studies on Cu(II), Co(II), Ni(II) complexes of Knoevenagel ß-diketone ligands.

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Green synthesis of gold nanoparticles using Trigonella foenum-graecum and its size-dependent catalytic activity.

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Synthesis and studies on Cu(II), Co(II), Ni(II) complexes of Knoevenagel ß-diketone ligands.

Content Provider	World Health Organization (WHO)-Global Index Medicus
Author	Sumathi, S. Tharmaraj, P. Sheela, C. D. Anitha, C.
Description	Country affiliation: India Author Affiliation: Sumathi S ( Department of Chemistry, Thiagarajar College, Madurai 625 009, India.)
Abstract	Transition metal complexes of various acetylacetone based ligands of the type ML [where M=Cu(II), Ni(II), Co(II); L=3-(aryl)-pentane-2,4-dione] have been synthesized. The structural features have been derived from their elemental analysis, magnetic susceptibility, molar conductance, IR, UV-Vis, (1)H NMR, Mass and ESR spectral studies. Conductivity measurements reveal that all the complexes are non-electrolytic in nature. Spectroscopic and other analytical data of the complexes suggest octahedral geometry for other metal(II) complexes. The redox behavior of the copper(II) complexes have been studied by cyclic voltammetry. The free ligands and their metal complexes have been screened for their in vitro biological activities against the bacteria Pseudomonas aeruginosa, Escherichia coli and Staphylococcus aureus as well as the fungus Candida albicans by well diffusion method. The zone of inhibition value indicates that the most of the metal(II) complexes are found to possess increased activities compared to those of the free ligands. All synthesized compounds may serve as potential photoactive materials as indicated from their characteristic fluorescence properties. The second harmonic generation (SHG) efficiency of the ligands (L1-L3) was found to be considerable effect than that of urea and KDP (potassium dihydrogen phosphate).
ISSN	13861425
Volume Number	97
e-ISSN	18733557
Journal	Spectrochimica Acta Part A: Molecular and Biomolecular Spectroscopy
Language	English
Publisher	Elsevier
Publisher Date	2012-11-01
Publisher Place	Great Britain (UK)
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	Coordination Complexes Chemistry Chemical Synthesis Ketones Bacteria Drug Effects Cobalt Pharmacology Copper Dimethyl Sulfoxide Electron Spin Resonance Spectroscopy Electrons Fungi Ligands Magnetic Phenomena Mass Spectrometry Microbial Sensitivity Tests Nickel Nonlinear Dynamics Oxidation-reduction Spectrometry, Fluorescence Spectrophotometry, Infrared Vibration Journal Article Research Support, Non-u.s. Gov't Discipline Spectroscopy
Content Type	Text
Resource Type	Article
Subject	Spectroscopy Atomic and Molecular Physics, and Optics Analytical Chemistry Instrumentation

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