NDLI: Coordination behavior of tetraaza [N4] ligand towards Co(II), Ni(II), Cu(II), Cu(I) and Pd(II) complexes: synthesis, spectroscopic characterization and anticancer activity.

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Coordination behavior of tetraaza [N4] ligand towards Co(II), Ni(II), Cu(II), Cu(I) and Pd(II) complexes: synthesis, spectroscopic characterization and anticancer activity.

Content Provider	World Health Organization (WHO)-Global Index Medicus
Author	El-Boraey, Hanaa A.
Description	Country affiliation: Egypt Author Affiliation: El-Boraey HA ( Department of Chemistry, Faculty of Science, El-Menoufia University, Shebin El-Kom, Egypt. helboraey@yahoo.com)
Abstract	Novel eight Co(II), Ni(II), Cu(II), Cu(I) and Pd(II) complexes with [N(4)] ligand (L) i.e. 2-amino-N-{2-[(2-aminobenzoyl)amino]ethyl}benzamide have been synthesized and structurally characterized by elemental analysis, spectral, thermal (TG/DTG), magnetic, and molar conductivity measurements. On the basis of IR, mass, electronic and EPR spectral studies an octahedral geometry has been proposed for Co(II), Ni(II) complexes and Cu(II) chloride complex, square-pyramidal for Cu(I) bromide complex. For Cu(II) nitrate complex (6), Pd(II) complex (8) square planar geometry was proposed. The EPR data of Cu(II) complexes in powdered form indicate d(x2-y2) ground state of Cu(II) ion. The antitumor activity of the synthesized ligand and some selected metal complexes has been studied. The palladium(II) complex (8) was found to display cytotoxicity (IC(50)=25.6 and 41 µM) against human breast cancer cell line MCF-7 and human hepatocarcinoma HEPG2 cell line.
ISSN	13861425
Volume Number	97
e-ISSN	18733557
Journal	Spectrochimica Acta Part A: Molecular and Biomolecular Spectroscopy
Language	English
Publisher	Elsevier
Publisher Date	2012-11-01
Publisher Place	Great Britain (UK)
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	Antineoplastic Agents Chemical Synthesis Pharmacology Aza Compounds Coordination Complexes Chemistry Cobalt Copper Differential Thermal Analysis Drug Screening Assays, Antitumor Electron Spin Resonance Spectroscopy Electrons Hep G2 Cells Humans Ligands Mcf-7 Cells Magnetic Phenomena Mass Spectrometry Nickel Palladium Spectrophotometry, Infrared Thermogravimetry X-ray Diffraction Journal Article Discipline Spectroscopy
Content Type	Text
Resource Type	Article
Subject	Spectroscopy Atomic and Molecular Physics, and Optics Analytical Chemistry Instrumentation

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