NDLI: Inâsitu studies of solvothermal synthesis of energy materials.

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Inâsitu studies of solvothermal synthesis of energy materials.

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Inâsitu studies of solvothermal synthesis of energy materials.

Content Provider	World Health Organization (WHO)-Global Index Medicus
Author	Jensen, Kirsten M. Ø. Tyrsted, Christoffer Bremholm, Martin Iversen, Bo B.
Description	Author Affiliation: Jensen KM ( Center for Materials Crystallography, Department of Chemistry and iNANO, Aarhus University, Langelandsgade 140, 8000 Aarhus C (Denmark) www.cmc.chem.au.dk.)
Abstract	Solvothermal and hydrothermal synthesis, that is, synthesis taking place in a solvent at elevated temperature and pressure, is a powerful technique for the production of advanced energy materials as it is versatile, cheap, and environmentally friendly. However, the fundamental reaction mechanisms dictating particle formation and growth under solvothermal conditions are not well understood. In order to produce tailor-made materials with specific properties for advanced energy technologies, it is essential to obtain an improved understanding of these processes and, in this context, inâsitu studies are an important tool as they provide real time information on the reactions taking place. Here, we present a review of the use of powder diffraction and total scattering methods for inâsitu studies of synthesis taking place under solvothermal and hydrothermal conditions. The experimental setups used for inâsitu X-ray and neutron studies are presented, and methods of data analysis are described. Special attention is given to the methods used to extract structural information from the data, for example, Rietveld refinement, whole powder pattern modelling and pair distribution function analysis. Examples of inâsitu studies are presented to illustrate the types of chemical insight that can be obtained.
File Format	HTM / HTML
ISSN	18645631
Issue Number	6
Volume Number	7
e-ISSN	1864564X
Journal	ChemSusChem
Language	English
Publisher	Wiley-VCH
Publisher Date	2014-06-01
Publisher Place	Germany
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	Electric Power Supplies Solvents Research Support, Non-u.s. Gov't Chemistry Temperature X-ray Diffraction Discipline Sustainable Chemistry Neutron Diffraction Review Powder Diffraction Journal Article
Content Type	Text
Resource Type	Article
Subject	Energy Environmental Chemistry Materials Science Chemical Engineering

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Inâsitu studies of solvothermal synthesis of energy materials.

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