NDLI: Comparative study of solution-phase and vapor-phase deposition of aminosilanes on silicon dioxide surfaces.

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Comparative study of solution-phase and vapor-phase deposition of aminosilanes on silicon dioxide surfaces.

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Year: 2013 Volume: 33

Year: 2012 Volume: 32

Comparative study of solution-phase and vapor-phase deposition of aminosilanes on silicon dioxide surfaces.

Content Provider	World Health Organization (WHO)-Global Index Medicus
Author	Yadav, Amrita R. Sriram, Rashmi Carter, Jared A. Miller, Benjamin L.
Description	Country affiliation: United States Author Affiliation: Yadav AR ( Department of Physics and Astronomy, University of Rochester, Rochester, NY, USA.); Sriram R ( Department of Biomedical Engineering, University of Rochester, Rochester, NY, USA.); Carter JA ( Adarza Biosystems, Inc., West Henrietta, NY, USA.); Miller BL ( Department of Biomedical Engineering, University of Rochester, Rochester, NY, USA)
Abstract	The uniformity of aminosilane layers typically used for the modification of hydroxyl bearing surfaces such as silicon dioxide is critical for a wide variety of applications, including biosensors. However, in spite of many studies that have been undertaken on surface silanization, there remains a paucity of easy-to-implement deposition methods reproducibly yielding smooth aminosilane monolayers. In this study, solution- and vapor-phase deposition methods for three aminoalkoxysilanes differing in the number of reactive groups (3-aminopropyl triethoxysilane (APTES), 3-aminopropyl methyl diethoxysilane (APMDES) and 3-aminopropyl dimethyl ethoxysilane (APDMES)) were assessed with the aim of identifying methods that yield highly uniform and reproducible silane layers that are resistant to minor procedural variations. Silane film quality was characterized based on measured thickness, hydrophilicity and surface roughness. Additionally, hydrolytic stability of the films was assessed via these thickness and contact angle values following desorption in water. We found that two simple solution-phase methods, an aqueous deposition of APTES and a toluene based deposition of APDMES, yielded high quality silane layers that exhibit comparable characteristics to those deposited via vapor-phase methods.
File Format	HTM / HTML
ISSN	09284931
e-ISSN	18730191
DOI	10.1016/j.msec.2013.11.017
Journal	Materials Science and Engineering: C
Volume Number	35
Language	English
Publisher	Elsevier
Publisher Date	2014-02-01
Publisher Place	Netherlands
Access Restriction	Open
Subject Keyword	Discipline Materials Science Coated Materials, Biocompatible Chemical Synthesis Silanes Chemistry Silicon Dioxide Adsorption Gases Hydrophobic And Hydrophilic Interactions Materials Testing Phase Transition Surface Properties Comparative Study Research Support, N.i.h., Extramural
Content Type	Text
Resource Type	Article
Subject	Mechanics of Materials Biomaterials Condensed Matter Physics Bioengineering Mechanical Engineering

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