NDLI: Evaluation of self-annealing behavior of electrodeposited silver film by EBSP analysis

Content Provider	IEEE Xplore Digital Library
Author	Hayashi, Yumi Shohji, Ikuo Miyazawa, Hiroshi
Copyright Year	2015
Description	Author affiliation: Faculty of Science and Technology, Gunma University 1-5-1, Tenjin-cho, Kiryu, Gunma 376-8515, Japan (Hayashi, Yumi; Shohji, Ikuo) \|\| DOWA METALTECH, Co., Ltd. 1781, Nitte, Honjo, Saitama 367-0002, Japan (Miyazawa, Hiroshi)
Abstract	Self-annealing behavior of an electrodeposited Ag film which has been preferentially oriented in (001) direction was investigated by electron backscatter diffraction pattern (EBSP) analysis. There are few clear grains of micrometer order in the initial state just after electrodepositing. The result shows that the electrodeposited film would be in amorphous state or could be consisted of very fine grains which size cannot be analyzed by EBSP. Self-annealing starts in storage at R.T. for a few hours and recrystallization almost completes in the storage time of 6 h. Recrystallized grains with relatively random orientation and a few micrometer order size have nucleate in storage time of a few hours. Afterward, (001) oriented grains preferentially grow in the self-annealing process. During self-annealing, the area fraction of (001) oriented grains increases rapidly and saturates in the range from 70 % to 80 % at the storage time over 6 h. The area fraction of (111) oriented grains slightly increases with increasing storage time, but it becomes at most 10 % even when self-annealing process has completed. On the contrary, the area fraction of (101) oriented grains decreases with increasing storage time and it becomes almost 0 % at the storage time over 6 h. Two patterns were found for formation of (001) oriented grains. One is that (001) orientation occurs at the same time as recrystallization and (001) oriented grains grow. In the other pattern, recrystallized grains oriented to near (001) in self-annealing process, subsequently the grains tilted from (001) are rotated to (001) by further storage.
Starting Page	1
Ending Page	4
File Size	989025
Page Count	4
File Format	PDF
e-ISBN	9781467372695
DOI	10.1109/EPTC.2015.7412286
Language	English
Publisher	Institute of Electrical and Electronics Engineers, Inc. (IEEE)
Publisher Date	2015-12-02
Publisher Place	Singapore
Access Restriction	Subscribed
Rights Holder	Institute of Electrical and Electronics Engineers, Inc. (IEEE)
Subject Keyword	Films Annealing Silver Grain size Plating Electronics packaging
Content Type	Text
Resource Type	Article

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4	Project PI / Joint PI	Principal Investigator and Joint Principal Investigators of the project	Dr. B. Sutradhar bsutra@ndl.gov.in Prof. Saswat Chakrabarti will be added soon
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