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| Content Provider | World Health Organization (WHO)-Global Index Medicus |
|---|---|
| Author | Wu, Zhi-Liang Liu, Qi Chen, Xiao-Qing Yu, Jin-Gang |
| Description | Country affiliation: China Author Affiliation: Wu ZL ( College of Chemistry and Chemical Engineering, Central South University, Changsha, Hunan, China.); Liu Q ( College of Chemistry and Chemical Engineering, Central South University, Changsha, Hunan, China.); Chen XQ ( College of Chemistry and Chemical Engineering, Central South University, Changsha, Hunan, China.); Yu JG ( Collaborative Innovation Center of Resource-conserving & Environment-friendly Society and Ecological Civilization, Changsha, Hunan, China.) |
| Abstract | A convenient and accurate analysis approach that combined solid-phase extraction and high-performance liquid chromatography was developed to determine the amount of Rhodamine B in red wine and Xiang-jiang river water samples. A novel composite, magnesium hydroxide/carbon nanotube composites, was synthesized and used as the solid-phase extractant for the preconcentration/analysis of Rhodamine B. Magnesium hydroxide/carbon nanotube composites, which combined the merits of carbon nanotubes and magnesium hydroxide, exhibited acceptable adsorption and desorption efficiencies for Rhodamine B. The linear range of the proposed solid-phase extraction with high-performance liquid chromatography method for Rhodamine B was 0.05-20.0 mg/L, with a limit of detection of 3.6 µg/L. The precision and reproducibility of the developed solid-phase extraction with high-performance liquid chromatography method and the batch-to-batch reproducibility of the solid-phase extractant were also validated at spiking levels of 0.5 and 2.0 mg/L. The recovery of Rhodamine B was 94.33-106.7%, and the recovery relative standard deviations of the intra- and interday precisions were ≤ 3.83 and ≤ 6.01%, respectively. The relative standard deviation of the batch-to-batch reproducibility was ≤ 7.98%. |
| File Format | HTM / HTML |
| ISSN | 16159306 |
| Issue Number | 19 |
| Journal | Journal of Separation Science |
| Volume Number | 38 |
| e-ISSN | 16159314 |
| Language | English |
| Publisher | Wiley-VCH |
| Publisher Date | 2015-10-01 |
| Publisher Place | Germany |
| Access Restriction | One Nation One Subscription (ONOS) |
| Content Type | Text |
| Resource Type | Article |
| Subject | Analytical Chemistry Filtration and Separation |
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