NDLI: Hair as a specimen to document tetramethylene disulfotetramine exposure.

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Hair as a specimen to document tetramethylene disulfotetramine exposure.

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Hair as a specimen to document tetramethylene disulfotetramine exposure.

Content Provider	World Health Organization (WHO)-Global Index Medicus
Author	Shen, Min Xiang, Ping Zhou, Fuxiang Shen, Baohua Shi, Yan
Spatial Coverage	China
Description	Author Affiliation: Shen M ( Department of Forensic Toxicology, Institute of Forensic Sciences, Ministry of Justice, Shanghai Key Laboratory of Forensic Medicine, Guangfu Xi Road 1347, Shanghai 200063, PR China.)
Abstract	Tetramethylene disulfotetramine (tetramine) is a rodenticide that has been banned for many years in China. Since 2005, inhabitants of a village in the Henan Province have been suffering from grand mal seizures. To investigate the possibility of tetramine as the cause, we developed a method to determine tetramine in human hair. Sample preparation involved external decontamination, frozen pulverization, and ultrasonication in 2 mL ethyl acetate in the presence of cocaine-d3 as an internal standard. The method exhibited good linearity; calibration curve was linear over a range of 0.1-20 ng/mg hair. The limit of detection for the assay was 0.05 ng/mg hair. Except for one subject (No. 4), all head and pubic hair samples were positive for tetramine. The concentrations of tetramine in pubic hair were significantly higher than those in the same subjects' head hair samples. Because of a long retention in body, segmental head hair analysis cannot provide an accurate exposure history of tetramine in the body.
File Format	HTM / HTML
ISSN	00221198
Issue Number	3
Volume Number	57
e-ISSN	15564029
Journal	Journal of Forensic Sciences
Language	English
Publisher	Wiley-Blackwell
Publisher Date	2012-05-01
Publisher Place	United States
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	Hair Research Support, Non-u.s. Gov't Rodenticides Adverse Effects Humans Middle Aged Gas Chromatography-mass Spectrometry Child, Preschool Male Discipline Forensic Sciences Forensic Toxicology Environmental Exposure Chemically Induced Journal Article Limit Of Detection Chemistry Bridged Compounds Analysis China Adult Female Child Epilepsy, Tonic-clonic
Content Type	Text
Resource Type	Article
Subject	Genetics Pathology and Forensic Medicine

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Hair as a specimen to document tetramethylene disulfotetramine exposure.

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