NDLI: Thermal desorption gas chromatography with mass spectrometry study of outgassing from polymethacrylimide foam (Rohacell®).

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Thermal desorption gas chromatography with mass spectrometry study of outgassing from polymethacrylimide foam (Rohacell®).

Content Provider	World Health Organization (WHO)-Global Index Medicus
Author	Carrasco-Correa, Enrique J. Herrero-Martínez, José M. Consuegra, Lina Ramis-Ramos, Guillermo Sanz, Rafael Mata Martínez, Benito Gimeno Esbert, Vicente E. Boria García-Baquero, David Raboso
Description	Country affiliation: Spain Author Affiliation: Carrasco-Correa EJ ( Department of Analytical Chemistry, Faculty of Chemistry, University of Valencia, Burjassot, Spain.); Herrero-Martínez JM ( Department of Analytical Chemistry, Faculty of Chemistry, University of Valencia, Burjassot, Spain.); Consuegra L ( Department of Analytical Chemistry, Faculty of Chemistry, University of Valencia, Burjassot, Spain.); Ramis-Ramos G ( Department of Analytical Chemistry, Faculty of Chemistry, University of Valencia, Burjassot, Spain.); Sanz RM ( Department of Applied Physics-ICMUV, Faculty of Physics, University of Valencia, Burjassot, Valencia, Spain.); Martínez BG ( Department of Applied Physics-ICMUV, Faculty of Physics, University of Valencia, Burjassot, Valencia, Spain.); Esbert VE ( Department of Communications-iTEAM, Polytechnic University of Valencia, Valencia, Spain.); García-Baquero DR ( European Space Agency, ESA/ESTEC, Noordwijk, The Netherlands.)
Abstract	Polymethacrylimide foams are used as light structural materials in outer-space devices; however, the foam closed cells contain volatile compounds that are outgassed even at low temperatures. These compounds ignite as plasmas under outer-space radiation and the intense radio-frequency fields used in communications. Since plasmas may cause spacecraft fatal events, the conditions in which they are ignited should be investigated. Therefore, qualitative and quantitative knowledge about polymethacrylimide foam outgassing should be established. Using thermogravimetric analysis, weight losses reached 3% at ca. 200°C. Thermal desorption gas chromatography with mass spectrometry detection was used to study the offgassed compounds. Using successive 4 min heating cycles at 125°C, each one corresponding to an injection, significant amounts of nitrogen (25.3%), water (2.6%), isobutylene (11.3%), tert-butanol (2.9%), 1-propanol (11.9%), hexane (25.3%), propyl methacrylate (1.4%), higher hydrocarbons (11.3%), fatty acids (2.2%) and their esters (1.3%), and other compounds were outgassed. Other compounds were observed during the main stage of thermal destruction (220-280°C). A similar study at 175°C revealed the extreme difficulty in fully outgassing polar compounds from polymethacrylimide foams by baking and showed the different compositions of the offgassed atmosphere that can be expected in the long term.
File Format	HTM / HTML
ISSN	16159306
Issue Number	17
Journal	Journal of Separation Science
Volume Number	38
e-ISSN	16159314
Language	English
Publisher	Wiley-VCH
Publisher Date	2015-09-01
Publisher Place	Germany
Access Restriction	One Nation One Subscription (ONOS)
Content Type	Text
Resource Type	Article
Subject	Analytical Chemistry Filtration and Separation

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