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Effects of calcination and support on supported manganese catalysts for the catalytic oxidation of toluene as a model of VOCs

Content Provider	Springer Nature Link
Author	Jung, Sang Chul Park, Young Kwon Jung, Ho Young Kang, Ung Il Nah, Jae Woon Kim, Sang Chai
Copyright Year	2015
Abstract	The conventional impregnation method was used to prepare 15 wt% Mn-supported catalysts, which were applied to the catalytic oxidation of volatile organic compounds (VOCs; toluene, benzene, and o-xylene). The effects of calcination temperatures in the range of 500–900 °C and supports (γ-Al$_{2}$O$_{3}$, SiO$_{2}$, and TiO$_{2}$) on the property and performance of 15 wt% Mn-supported catalysts were investigated. Their physicochemical characteristics were analyzed by the BET, XRD, NH$_{3}$–TPD, H$_{2}$–TPR, and XPS. The calcination temperature greatly affected the crystalline structure and O1s $_{D}$ (defect oxides)/O1s $_{L}$ (lattice oxides) area ratio of the 15 wt% Mn/γ-Al$_{2}$O$_{3}$ (15 Mn/Al) catalyst. The order of the O1s $_{D}$/O1s $_{L}$ area ratios of the 15 Mn/Al catalysts with respect to calcination temperature was 900 > 500 > 700 °C, which was in good agreement with that observed for the catalytic activity. In addition, the activity order of the 15 wt% Mn-supported catalysts with respect to the type of support was γ-Al$_{2}$O$_{3}$ > SiO$_{2}$ > TiO$_{2}$. The 15 wt% Mn/Al catalyst, which had a higher O1s $_{D}$/O1s $_{L}$ area ratio, showed better activity than the 15 wt% Mn/SiO$_{2}$ (15 Mn/Si) and 15 wt% Mn/TiO$_{2}$ (15 Mn/Ti) catalysts. Defect oxides played a significant role in the catalytic oxidation of VOCs. The catalytic activity with respect to the type of VOC decreased in the order of benzene > toluene > o-xylene.
Starting Page	185
Ending Page	199
Page Count	15
File Format	PDF
ISSN	09226168
Journal	Research on Chemical Intermediates
Volume Number	42
Issue Number	1
e-ISSN	15685675
Language	English
Publisher	Springer Netherlands
Publisher Date	2015-12-12
Publisher Place	Dordrecht
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	Catalytic oxidation Volatile organic compounds Calcination temperature Manganese Support Catalysis Physical Chemistry Inorganic Chemistry
Content Type	Text
Resource Type	Article
Subject	Chemistry

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