NDLI: Domain and antiferroelectric properties of Pb(Lu1/2Nb1/2)O3 single crystals and their superlattice structure

Content Provider	Royal Society of Chemistry (RSC)
Author	Wang, Zujian Liu, Ying Long, Xifa He, Chao Yang, Xiaoming Li, Xiuzhi Xiao, Yuzhe
Copyright Year	2017
Abstract	In order to obtain antiferroelectric single crystals for understanding their structure and the physics and chemistry of the antiferroelectric phenomenon, antiferroelectric single crystals of Pb(Lu1/2Nb1/2)O3 (PLN) were successfully grown. Two sets of superlattice reflections including the B-site atom ordering type reflection and the lead-ion antiparallel ordering type reflection were confirmed and distinguished from the X-ray diffraction patterns and transmission electron microscopy. Micro-domains and macro-domains were observed under the microscopes. The investigations were focused on the extinction angle, the angle of the domain wall and temperature dependence. The Curie temperature TC was about 240 °C and 254 °C for [111]-oriented and [001]-oriented crystal plates respectively. The value of the energy density was calculated to be 3.65 J cm−3 for the [111]-oriented sample at 200 °C based on the double hysteresis loops with an electric field EAPP = 170 kV cm−1 applied. All the above features, especially the high Curie temperature and high energy storage density, suggested that the PLN single crystals should be useful for large size energy storage devices that require a wider operation temperature range.
Starting Page	3704
Ending Page	3712
Page Count	9
File Format	HTM / HTML PDF
ISSN	20462069
Volume Number	7
Issue Number	7
Journal	RSC Advances
DOI	10.1039/c6ra26171j
Language	English
Publisher	Royal Society of Chemistry
Access Restriction	Open
Subject Keyword	Extinction (optical mineralogy) Energy density Domain wall Physics Curie temperature X-ray crystallography Computational chemistry Transmission electron microscopy Electric field Lead Curie Correlation and dependence Superlattice Hysteresis
Content Type	Text
Resource Type	Article
Subject	Chemistry Chemical Engineering

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