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Rapid determination of nine haloacetic acids in water using ultra-performance liquid chromatography-tandem mass spectrometry in multiple reactions monitoring mode

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Analytical Methods Vol - 3 Issue - 6

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Analytical Methods Vol -1

Rapid determination of nine haloacetic acids in water using ultra-performance liquid chromatography-tandem mass spectrometry in multiple reactions monitoring mode

Content Provider	Royal Society of Chemistry (RSC)
Author	Mulcahy, Dennis Si, Jia Li, Wei Duan, Jinming
Copyright Year	2011
Abstract	A simple and rapid detection method for nine haloacetic acids (HAAs) in water has been developed using ultra-performance liquid chromatography-electrospray ionization tandem mass spectrometry (UPLC-ESI-MS/MS) in multiple reactions monitoring (MRM) mode. Addition of a small amount of formic acid (FA) as a modifier for the methanol–water eluent was found to be critical for separation of the analytes with smaller molecular size (i.e. the mono and di-haloacetic acids). Without the need of sample preconcentration, very low limits of detection (LODs) for the nine HAAs were achieved (0.06–0.16 μg L−1). The linear calibration range extended from 0.5 up to 100 μg L−1 (R2 = 0.9993–0.9997, n = 6). The water matrix effect has been examined, and seems to be related to the ions in real water samples. Interestingly, an adjustment of the pH of the tap water samples to an acidic value of 3 or below basically eliminated the matrix effect. The method has been tested using tap water samples sourced from both surface water (total dissolved solid (TDS): 145 ± 3 mg L−1) and groundwater (TDS: 362 ± 1 mg L−1) with high precision and recovery. A separation mechanism of the ionic analytes using a reversed phase liquid chromatographic column (HSS T3) possessing a hydrophilic affinity has been proposed and discussed.
Starting Page	1667
Ending Page	1673
Page Count	7
File Format	HTM / HTML PDF
ISSN	17599660
Volume Number	3
Issue Number	7
Journal	Analytical Methods
DOI	10.1039/c1ay05122a
Language	English
Publisher	Royal Society of Chemistry
Access Restriction	Open
Subject Keyword	Haloacetic acids Acid Elution Groundwater Ionization PH Hydrophile Mass spectrometry Chromatography
Content Type	Text
Resource Type	Article
Subject	Analytical Chemistry Engineering Chemical Engineering

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