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Evaluating the performance of three GC columns commonly used for the analysis of ignitable liquid mixtures encountered in fire debris

Content Provider	Royal Society of Chemistry (RSC)
Author	Choodum, Aree Daeid, Niamh Nic
Copyright Year	2011
Abstract	The analysis of debris recovered from fire scenes for the presence of ignitable liquids is of increasing importance for fire scene investigation. Increasingly this is carried out using Gas chromatography-mass spectroscopy (GCMS) using a standard dimethylpolysiloxane capillary column. Various publications in the available literature and survey data from forensic science laboratories favour HP-1 or HP-5 columns or their equivalent but no direct comparison of the sensitivity, selectivity or resolution of these columns for test mixtures relevant to ignitable liquid matrices have been published. This present work addresses this by analysing a matrix matched test mixture and an ignitable liquid test mixture using three different commercially available dimethylpolysiloxane columns currently referenced in the literature for ignitable liquid analysis. The ASTM standard method for analysis of ignitable liquids using GCMS was adopted and systematically modified for each column to afford maximum separation of the analytes and the results are presented.
Starting Page	1525
Ending Page	1534
Page Count	10
File Format	HTM / HTML PDF
ISSN	17599660
Volume Number	3
Issue Number	7
Journal	Analytical Methods
DOI	10.1039/c1ay05048f
Language	English
Publisher	Royal Society of Chemistry
Access Restriction	Open
Subject Keyword	Spectroscopy Forensic science ASTM Hewlett-Packard ASTM International Composite material
Content Type	Text
Resource Type	Article
Subject	Analytical Chemistry Engineering Chemical Engineering

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Detection and Characterization of Ignitable Liquid Residues in Forensic Fire Debris Samples by Comprehensive Two-Dimensional Gas Chromatography

Astm standards for fire debris analysis: a review (2002).

Identification of Ignitable Liquid Residues in Fire Debris by GC/MS/MS

Developing a Method for the Collection and Analysis of Burnt Remains for the Detection and Identification of Ignitable Liquid Residues Using Body Bags, Dynamic Headspace Sampling, and TD-GC×GC-TOFMS

Evaluation of an untargeted chemometric approach for the source inference of ignitable liquids in forensic science

Discrimination of Ignitable Liquid Residues in Burned Petroleum-Derived Substrates by Using HS-MS eNose and Chemometrics

Field test kits for collection of ignitable liquids and ignitable liquid residues used by the NSW fire scene investigators.

Fire behavior computations with the hewlett-packard hp-71 b calculator (1986).

Effects of Fire Suppression Agents and Weathering in the Analysis of Fire Debris by HS-MS eNose

Evaluating the performance of three GC columns commonly used for the analysis of ignitable liquid mixtures encountered in fire debris

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Detection and Characterization of Ignitable Liquid Residues in Forensic Fire Debris Samples by Comprehensive Two-Dimensional Gas Chromatography

Astm standards for fire debris analysis: a review (2002).

Identification of Ignitable Liquid Residues in Fire Debris by GC/MS/MS

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Evaluating the performance of three GC columns commonly used for the analysis of ignitable liquid mixtures encountered in fire debris