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| Content Provider | IEEE Xplore Digital Library |
|---|---|
| Author | Fujieda, S. Shinoda, K. Suzuki, S. Jeyadevan, B. |
| Copyright Year | 1965 |
| Abstract | The ordering process of FePt nanoparticles synthesized in polyol solution at 383 K was investigated. Whereas X-ray diffraction peaks of the as-synthesized specimen corresponded to the fcc structure, the Fe-O correlation and Pt-O correlation peaks were observed in the radial structure functions of Fe and Pt atoms obtained by X-ray absorption spectroscopy. Thus, the as-synthesized specimen was composed of crystalline FePt alloy phase and poorly crystallized Fe- and Pt-oxide phase. In X-ray diffraction patterns of the specimens which were heat-treated at temperatures above 568 K in a mixture of 5%H2 in Ar, diffraction peaks corresponding to superlattice lines were observed. Although the lattice constants of the as-synthesized specimen were much larger than that of the bulk fcc-FePt alloy with equiatomic composition, the lattice constants of the specimen heat-treated at 1173 K were very close to the bulk L10-FePt alloy. Additionally, in the radial structure function, peaks corresponding to the Fe-O and Pt-O correlations disappeared and peaks corresponding to Fe-Pt (or Fe) and Pt-Fe (Pt) correlations clearly appeared after heat treatment at temperatures above 568 K. Consequently, it is highly probable that the disorder-order transformation of FePt nanoparticles synthesized in polyol solution is accompanied by compositional homogenization due to the reduction of the poorly crystallized Fe- and Pt-oxide phase. |
| Sponsorship | IEEE Magnetics Society |
| Starting Page | 3303 |
| Ending Page | 3306 |
| Page Count | 4 |
| File Size | 606408 |
| File Format | |
| ISSN | 00189464 |
| Volume Number | 49 |
| Issue Number | 7 |
| Language | English |
| Publisher | Institute of Electrical and Electronics Engineers, Inc. (IEEE) |
| Publisher Date | 2013-07-01 |
| Publisher Place | U.S.A. |
| Access Restriction | One Nation One Subscription (ONOS) |
| Rights Holder | Institute of Electrical and Electronics Engineers, Inc. (IEEE) |
| Subject Keyword | Nanoparticles Heat treatment Iron Absorption Heating X-ray diffraction polyol process EXAFS L1$_{0}$-type structure local structure |
| Content Type | Text |
| Resource Type | Article |
| Subject | Electronic, Optical and Magnetic Materials Electrical and Electronic Engineering |
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