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| Content Provider | World Health Organization (WHO)-Global Index Medicus |
|---|---|
| Author | Ahmed, Ibrahim S. Moustafa, Moustafa M. Abd El Aziz, Mohamed M. |
| Description | Country affiliation: Egypt Author Affiliation: Ahmed IS ( Chemistry Department, Faculty of Science, Benha University, Benha City, Egypt. isahmed2010@gmail.com) |
| Abstract | New azo-azomethine dyes were prepared by reaction of p-aminobenzoic acid, o-anisidine, o-nitroaniline, and p-bromoaniline with salicylaldehyde respectively to form azo compounds and then condensation by urea to form 4-(R-arylazo 2-salicylaldene)-urea azo-azomethine derivatives (I(a-d)). The complexes of these ligands with Ag(I), Cu(II), Zn(II) and Hg(II) metal ions were prepared. The structure of the free ligands and their complexes were characterized by using elemental analysis (C, H, N), (1)H NMR, IR and UV-Vis-spectra. The proton dissociation constants of the ligands and the stability constant of their complexes have been determined potentiometrically in 40% (v/v) alcohol-water medium as well as the stoichiometry of complexes were determined conductometrically. The data reveal that the stoichiometries for all complexes were prepared in molar ratios (1:1) and (1:2) (M:L). The electrolytic and nonelectrolytic natures of the complexes were assigned based on molar conductance measurements. The thermogravimetric (TG), and differential thermal analyses (DTA) were studied in nitrogen atmosphere with heating rate 10°C/min. The kinetic and thermodynamic parameters for thermal decomposition of complexes have been calculated by graphical method using Coats-Redfern (CR) method. |
| ISSN | 13861425 |
| Issue Number | 5 |
| Volume Number | 78 |
| e-ISSN | 18733557 |
| Journal | Spectrochimica Acta Part A: Molecular and Biomolecular Spectroscopy |
| Language | English |
| Publisher | Elsevier |
| Publisher Date | 2011-05-01 |
| Publisher Place | Great Britain (UK) |
| Access Restriction | One Nation One Subscription (ONOS) |
| Subject Keyword | Azo Compounds Chemistry Chemical Synthesis Metals, Heavy Potentiometry Methods Temperature Thiosemicarbazones Conductometry Copper Electric Conductivity Electrons Kinetics Ligands Magnetic Resonance Spectroscopy Mercury Protons Silver Spectrophotometry, Infrared Thermogravimetry Zinc Journal Article Discipline Spectroscopy |
| Content Type | Text |
| Resource Type | Article |
| Subject | Spectroscopy Atomic and Molecular Physics, and Optics Analytical Chemistry Instrumentation |
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