NDLI: Rapid thermal processing chamber for in-situ x-ray diffraction.

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Invited article: A round robin test of the uncertainty on the measurement of the thermoelectric dimensionless figure of merit of Co0.97Ni0.03Sb3.

Contributed review: Review of integrated correlative light and electron microscopy.

System for measuring temporal profiles of scintillation at high and different linear energy transfers by using pulsed ion beams.

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Analysis and calibration techniques for superconducting resonators.

Fibre optics wavemeters calibration using a self-referenced optical frequency comb.

Fast temperature spectrometer for samples under extreme conditions.

A new facility for the synchrotron radiation-based calibration of transfer radiation sources in the ultraviolet and vacuum ultraviolet spectral range.

Optical microscope and tapered fiber coupling apparatus for a dilution refrigerator.

Temperature cross-sensitivity characteristics of singlemode-multimode-singlemode fiber structure.

A compact electron gun for time-resolved electron diffraction.

Reflective multilayer optic as hard X-ray diagnostic on laser-plasma experiment.

Time-resolved spectroscopy using a chopper wheel as a fast shutter.

A home-made system for IPCE measurement of standard and dye-sensitized solar cells.

Operating single quantum emitters with a compact Stirling cryocooler.

Collimated electron beam accelerated at 12 kV from a Penning discharge.

Stretched arc discharge in produced water.

Research on anisotropy of fusion-produced protons and neutrons emission from high-current plasma-focus discharges.

Experimental investigation of a 1 kA/cm² sheet beam plasma cathode electron gun.

Analysis of double-probe characteristics in low-frequency gas discharges and its improvement.

Precise and direct method for the measurement of the torsion spring constant of the atomic force microscopy cantilevers.

Two-dimensional scanning focused refractive-index microscopy and applications to refractive-index profiling of optical fibers.

Correction of absorption-edge artifacts in polychromatic X-ray tomography in a scanning electron microscope for 3D microelectronics.

A simple compact UHV and high magnetic field compatible inertial nanopositioner.

Mapping of ferroelectric domain structure using angle-resolved piezoresponse force microscopy.

Three axis vector magnet set-up for cryogenic scanning probe microscopy.

High-speed microscopy with an electrically tunable lens to image the dynamics of in vivo molecular complexes.

Instrument for evaluating the electrical resistance and wavelength-resolved transparency of stretchable electronics during strain.

Rapid thermal processing chamber for in-situ x-ray diffraction.

Multilayer film shields for the protection of PMT from constant magnetic field.

High-throughput on-the-fly scanning ultraviolet-visible dual-sphere spectrometer.

High-bandwidth, high-sampling-rate, low-noise, two-probe transient photovoltage measuring system.

Spectral restoration in high resolution electron energy loss spectroscopy based on iterative semi-blind Lucy-Richardson algorithm applied to rutile surfaces.

Fiber-fed time-resolved photoluminescence for reduced process feedback time on thin-film photovoltaics.

Momentum resolution in inverse photoemission.

A flexible experimental setup for femtosecond time-resolved broad-band ellipsometry and magneto-optics.

Fourier transform two-dimensional fluorescence excitation spectrometer by using tandem Fabry-Pérot interferometer.

gLISA: geosynchronous laser interferometer space antenna concepts with off-the-shelf satellites.

A compact 100 kV high voltage glycol capacitor.

Instrument for in-situ orientation of superconducting thin-film resonators used for electron-spin resonance experiments.

Development of an S-band cavity-type beam position monitor for a high power THz free-electron laser.

Calibration-independent measurement of complex permittivity of liquids using a coaxial transmission line.

A 90° fair circular waveguide bend.

Laser flash-Raman spectroscopy method for the measurement of the thermal properties of micro/nano wires.

Optical layer development for thin films thermal conductivity measurement by pulsed photothermal radiometry.

Nanogram calorimetry using microscale suspended SiNx platforms fabricated via focused ion beam patterning.

Raman measurements of substrate temperature in a molecular beam epitaxy growth chamber.

Reusable bi-directional 3ω sensor to measure thermal conductivity of 100-µm thick biological tissues.

Development of modulated optical transmission system to determinate the cloud and freezing points in biofuels.

Automatic droplet transportation on a plastic microfluidic device having wettability gradient surface.

Sensing of fluid viscoelasticity from piezoelectric actuation of cantilever flexural vibration.

Ultrasonic technique for monitoring of liquid density variations.

A portable automatic pressure delivery system for scar compression therapy in large animals.

Design of an ultrashort optical transmission cell for vacuum ultraviolet spectroscopy of supercritical fluids.

A novel system for measurement of the transverse electron momentum distribution from photocathodes.

A new phase difference measurement algorithm for extreme frequency signals based on discrete time Fourier transform with negative frequency contribution.

Development of an aerodynamic measurement system for hypersonic rarefied flows.

On precise phase difference measurement approach using border stability of detection resolution.

Instrument for spatially resolved simultaneous measurements of forces and currents in particle beams.

Coating thermal diffusivity and effusivity measurement optimization using regression-based sensitivity.

A large-dynamic-range current probe for microsecond pulsed vacuum breakdown research.

Combined alternating gradient force magnetometer and susceptometer system.

Ultraprecision XY stage using a hybrid bolt-clamped Langevin-type ultrasonic linear motor for continuous motion.

Method and apparatus for characterization of electric field-induced aggregation in pre-crystalline protein solutions.

Note: Liquid chemical sensing by emission spectroscopy with a nanosecond pin-hole discharge in water.

Note: A stand on the basis of atomic force microscope to study substrates for imaging optics.

Note: A microfluidic freezer based on evaporative cooling of atomized aqueous microdroplets.

Note: A pulsed laser ion source for linear induction accelerators.

Note: Experimental platform for magnetized high-energy-density plasma studies at the omega laser facility.

Note: Inter-satellite laser range-rate measurement by using digital phase locked loop.

Note: Improved wire-wound heater.

Note: A novel trigger generator for a pseudospark switch.

Note: A balloon-borne accelerometer technique for measuring atmospheric turbulence.

Note: O-ring stack system for electron gun alignment.

Note: Position dependence of time signals picked off a microchannel plate detector.

Note: Fabrication and characterization of molybdenum tips for scanning tunneling microscopy and spectroscopy.

Note: A 95 GHz mid-power gyrotron for medical applications measurements.

Note: Effect of hot liner in producing 40,48Ca beam from RIKEN 18-GHz electron cyclotron resonance ion source.

Note: Sample cells to investigate solid/liquid interfaces with neutrons.

Note: The design of thin gap chamber simulation signal source based on field programmable gate array.

Note: An improved driver section for a diaphragmless shock tube.

Note: Eddy current displacement sensors independent of target conductivity.

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Rapid thermal processing chamber for in-situ x-ray diffraction.

Content Provider	World Health Organization (WHO)-Global Index Medicus
Author	Toney, Michael F. Parilla, Philip A. Fields, Jeremy D. Pool, Vanessa L. Ahmad, Md Imteyaz Yu, Jiafan Van Hest, Maikel F. A. M. Van Campen, Douglas G. Ginley, David S.
Description	Country affiliation: United States Author Affiliation: Ahmad MI ( SSRL, SLAC National Accelerator Laboratory, 2575, Sand Hill Road, Menlo Park, California 94025, USA.); Van Campen DG ( SSRL, SLAC National Accelerator Laboratory, 2575, Sand Hill Road, Menlo Park, California 94025, USA.); Fields JD ( National Renewable Energy Laboratory, Golden, Colorado 80401, USA.); Yu J ( SSRL, SLAC National Accelerator Laboratory, 2575, Sand Hill Road, Menlo Park, California 94025, USA.); Pool VL ( SSRL, SLAC National Accelerator Laboratory, 2575, Sand Hill Road, Menlo Park, California 94025, USA.); Parilla PA ( National Renewable Energy Laboratory, Golden, Colorado 80401, USA.); Ginley DS ( National Renewable Energy Laboratory, Golden, Colorado 80401, USA.); Van Hest MF ( SSRL, SLAC National Accelerator Laboratory, 2575, Sand Hill Road, Menlo Park, California 94025, USA.); Toney MF ( SSRL, SLAC National Accelerator Laboratory, 2575, Sand Hill Road, Menlo Park, California 94025, USA.)
Abstract	Rapid thermal processing (RTP) is widely used for processing a variety of materials, including electronics and photovoltaics. Presently, optimization of RTP is done primarily based on ex-situ studies. As a consequence, the precise reaction pathways and phase progression during the RTP remain unclear. More awareness of the reaction pathways would better enable process optimization and foster increased adoption of RTP, which offers numerous advantages for synthesis of a broad range of materials systems. To achieve this, we have designed and developed a RTP instrument that enables real-time collection of X-ray diffraction data with intervals as short as 100 ms, while heating with ramp rates up to 100 °Cs(-1), and with a maximum operating temperature of 1200 °C. The system is portable and can be installed on a synchrotron beamline. The unique capabilities of this instrument are demonstrated with in-situ characterization of a Bi2O3-SiO2 glass frit obtained during heating with ramp rates 5 °C s(-1) and 100 °C s(-1), revealing numerous phase changes.
ISSN	00346748
Issue Number	1
Journal	Review of Scientific Instruments
Volume Number	86
e-ISSN	10897623
Language	English
Publisher	American Institute of Physics
Publisher Date	2015-01-01
Publisher Place	United States
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	Discipline Physics Discipline Chemistry
Content Type	Text
Resource Type	Article
Subject	Medicine Instrumentation

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