NDLI: The large volume press facility at ID06 beamline of the European synchrotron radiation facility as a High Pressure-High Temperature deformation apparatus.

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The large volume press facility at ID06 beamline of the European synchrotron radiation facility as a High Pressure-High Temperature deformation apparatus.

A lab-based ambient pressure x-ray photoelectron spectrometer with exchangeable analysis chambers.

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Publisher's Note: 'New developments in micro-X-ray diffraction and X-ray absorption spectroscopy for high-pressure research at 16-BM-D at the Advanced Photon Source' [Rev. Sci. Instrum. 86, 072205 (2015)].

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The large volume press facility at ID06 beamline of the European synchrotron radiation facility as a High Pressure-High Temperature deformation apparatus.

Content Provider	World Health Organization (WHO)-Global Index Medicus
Author	Crichton, Wilson A. Guignard, Jeremy
Description	Country affiliation: France Author Affiliation: Guignard J ( European Synchrotron Radiation Facility, 6 Rue Jules Horowitz, 38000 Grenoble, France.); Crichton WA ( European Synchrotron Radiation Facility, 6 Rue Jules Horowitz, 38000 Grenoble, France.)
Abstract	We report here the newly developed deformation setup offered by the 20MN (2000T) multi-anvil press newly installed at sector 7 of the European synchrotron radiation facility, on the ID06 beamline. The press is a Deformation-DIA (D-DIA) type apparatus, and different sets of primary anvils can be used for deformation experiments, from 6 mm to 3 mm truncations, according to the target pressure needed. Pressure and temperature calibrations and gradients show that the central zone of the assemblies is stable. Positions of differential RAMs are controlled with a sub-micron precision allowing strain rate from 10(-4) to 10(-6) s(-1). Moreover, changing differential RAM velocity is immediately visible on sample, making faster reaching of steady state. Lattice stresses are determined by the shifting of diffraction peak with azimuth angle using a linear detector covering typically a 10° solid-angle in 2Î¸ mounted on rotation perpendicular to the beam. Acquisition of diffraction pattern, at a typical energy of 55 keV, is less than a minute to cover the whole azimuth-2Î¸ space. Azimuth and d-spacing resolution are respectively better than 1° and 10(-3) Å making it possible to quantify lattice stresses with a precision of ±20 MPa (for silicates, which have typically high values of elastic properties), in pure or simple shear deformation measurements. These mechanical data are used to build fully constrained flow laws by varying P-T-σ-ÎµÌ conditions with the aim to better understanding the rheology of Earth's mantle. Finally, through texture analysis, it is also possible to determine lattice preferred orientation during deformation by quantifying diffraction peak intensity variation with azimuth angle. This press is therefore included as one of the few apparatus that can perform such experiments combining with synchrotron radiation.
ISSN	00346748
Issue Number	8
Journal	Review of Scientific Instruments
Volume Number	86
e-ISSN	10897623
Language	English
Publisher	American Institute of Physics
Publisher Date	2015-08-01
Publisher Place	United States
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	Discipline Physics Discipline Chemistry
Content Type	Text
Resource Type	Article
Subject	Medicine Instrumentation

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