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| Content Provider | World Health Organization (WHO)-Global Index Medicus |
|---|---|
| Author | Martín-Esteban, Antonio Barahona, Francisco Díaz-Álvarez, Myriam Turiel, Esther |
| Description | Country affiliation: Spain Author Affiliation: Barahona F ( Departamento de Medio Ambiente, INIA, Carretera de A Coruña km 7.5, 28040 Madrid, Spain.); Díaz-Álvarez M ( Departamento de Medio Ambiente, INIA, Carretera de A Coruña km 7.5, 28040 Madrid, Spain.); Turiel E ( Departamento de Medio Ambiente, INIA, Carretera de A Coruña km 7.5, 28040 Madrid, Spain.); Martín-Esteban A ( Departamento de Medio Ambiente, INIA, Carretera de A Coruña km 7.5, 28040 Madrid, Spain. Electronic address: amartin@inia.es.) |
| Abstract | In this work, novel molecularly imprinted polymer-coated hollow fibers (MIP-HFs) have been prepared and evaluated for the development of a micro-solid phase extraction method for the analysis of triazines in aqueous samples using high performance liquid chromatography and UV detection. The proposed extraction method combines liquid-liquid microextraction and molecular imprinting technology. In brief, a thin film of toluene is immobilised in the pores of the obtained MIP-HF. Afterwards, the conditioned MIP-HF is immersed in the water sample. Under stirring for a certain time, the target analytes are liquid-liquid extracted from the sample to the immobilised toluene and then these diffuse to the specific binding sites of the MIP. The effect of various experimental parameters as time and stirring-rate and salting-out effect among others, were studied for the establishment of optimum rebinding conditions. Recoveries for seven triazines tested in 100mL pure water samples spiked with 15 µg L(-1) of each triazine were within 0.8-6.9%, with a relative standard deviation (RSD)<10% (n=3). The detection limits (LODs) were within 0.05-0.1 µg L(-1), depending upon the triazine. The proposed methodology was successfully applied to extract the triazines from spiked tap and river water samples at µg L(-1) concentration level. The mircroextraction procedure with the developed MIP-HFs overcomes the typical low performance and lack of selective recognition of MIPs in aqueous media, allowing the determination of triazines in environmental waters at expected real concentration levels. |
| ISSN | 00219673 |
| Volume Number | 1442 |
| e-ISSN | 18733778 |
| Journal | Journal of Chromatography A |
| Language | English |
| Publisher | Elsevier |
| Publisher Date | 2016-04-15 |
| Publisher Place | Netherlands |
| Access Restriction | One Nation One Subscription (ONOS) |
| Subject Keyword | Environmental Monitoring Methods Fresh Water Chemistry Polymers Triazines Analysis Isolation & Purification Chromatography, High Pressure Liquid Limit Of Detection Liquid Phase Microextraction Molecular Imprinting Solid Phase Extraction Toluene Water Pollutants, Chemical Journal Article Research Support, Non-u.s. Gov't Discipline Analytical Chemistry |
| Content Type | Text |
| Resource Type | Article |
| Subject | Organic Chemistry Medicine Analytical Chemistry Biochemistry |
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