NDLI: Simultaneous determination of multiclass emerging contaminants in aquatic plants by ultrasound-assisted matrix solid-phase dispersion and GC-MS

Content Provider	Springer Nature Link
Author	Aznar, Ramón Albero, Beatriz Sánchez Brunete, Consuelo Miguel, Esther Martín Girela, Isabel Tadeo, José L.
Copyright Year	2016
Abstract	A multiresidue method was developed for the simultaneous determination of 31 emerging contaminants (pharmaceutical compounds, hormones, personal care products, biocides, and flame retardants) in aquatic plants. Analytes were extracted by ultrasound-assisted matrix solid-phase dispersion (UA-MSPD) and determined by gas chromatography-mass spectrometry after sylilation, The method was validated for different aquatic plants (Typha angustifolia, Arundo donax, and Lemna minor) and a semiaquatic cultivated plant (Oryza sativa) with good recoveries at concentrations of 100 and 25 ng g$^{−1}$ wet weight, ranging from 70 to 120 %, and low method detection limits (0.3 to 2.2 ng g$^{−1}$ wet weight). A significant difference of the chromatographic response was observed for some compounds in neat solvent versus matrix extracts, and therefore, quantification was carried out using matrix-matched standards in order to overcome this matrix effect. Aquatic plants taken from rivers located at three Spanish regions were analyzed, and the compounds detected were parabens, bisphenol A, benzophenone-3, cyfluthrin, and cypermethrin. The levels found ranged from 6 to 25 ng g$^{−1}$ wet weight except for cypermethrin that was detected at 235 ng g$^{−1}$ wet weight in O. sativa samples.
Starting Page	7911
Ending Page	7920
Page Count	10
File Format	PDF
ISSN	09441344
Journal	Environmental Science and Pollution Research
Volume Number	24
Issue Number	9
e-ISSN	16147499
Language	English
Publisher	Springer Berlin Heidelberg
Publisher Date	2016-02-24
Publisher Place	Berlin, Heidelberg
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	Aquatic plants Ultrasound-assisted matrix solid-phase dispersion GC-MS Emerging contaminants Typha angustifolia Oryza sativa Pharmaceuticals Biocides Environment Environmental Chemistry Ecotoxicology Environmental Health Atmospheric Protection/Air Quality Control/Air Pollution Waste Water Technology Water Pollution Control Water Management Aquatic Pollution
Content Type	Text
Resource Type	Article
Subject	Environmental Chemistry Health, Toxicology and Mutagenesis Pollution Medicine

Sl.	Authority	Responsibilities	Communication Details
1	Ministry of Education (GoI), Department of Higher Education	Sanctioning Authority	https://www.education.gov.in/ict-initiatives
2	Indian Institute of Technology Kharagpur	Host Institute of the Project: The host institute of the project is responsible for providing infrastructure support and hosting the project	https://www.iitkgp.ac.in
3	National Digital Library of India Office, Indian Institute of Technology Kharagpur	The administrative and infrastructural headquarters of the project	Dr. B. Sutradhar bsutra@ndl.gov.in
4	Project PI / Joint PI	Principal Investigator and Joint Principal Investigators of the project	Dr. B. Sutradhar bsutra@ndl.gov.in Prof. Saswat Chakrabarti will be added soon
5	Website/Portal (Helpdesk)	Queries regarding NDLI and its services	support@ndl.gov.in
6	Contents and Copyright Issues	Queries related to content curation and copyright issues	content@ndl.gov.in
7	National Digital Library of India Club (NDLI Club)	Queries related to NDLI Club formation, support, user awareness program, seminar/symposium, collaboration, social media, promotion, and outreach	clubsupport@ndl.gov.in
8	Digital Preservation Centre (DPC)	Assistance with digitizing and archiving copyright-free printed books	dpc@ndl.gov.in
9	IDR Setup or Support	Queries related to establishment and support of Institutional Digital Repository (IDR) and IDR workshops	idr@ndl.gov.in

Determination of phenols and pharmaceuticals in municipal wastewaters from Polish treatment plants by ultrasound-assisted emulsification–microextraction followed by GC–MS

Monitoring pharmaceuticals and personal care products in reservoir water used for drinking water supply

Analytical method development for the determination of eight biocides in various environmental compartments and application for monitoring purposes

Detection of Benzo[a]pyrene in Fried Food by Ultrasound-Assisted Matrix Solid-Phase Dispersion and Isotope Dilution GC–MS

Temporal variation of heavy metal accumulation and translocation characteristics of narrow-leaved cattail (Typha angustifolia L.)

Prioritisation of organic contaminants in a river basin using chemical analyses and bioassays

A 3-year study on occurrence of emerging contaminants in an urban stream of São Paulo State of Southeast Brazil

New trends in the analytical determination of emerging contaminants and their transformation products in environmental waters

Presence of Pharmaceuticals and Hormones in Waters from Sewage Treatment Plants

Simultaneous determination of multiclass emerging contaminants in aquatic plants by ultrasound-assisted matrix solid-phase dispersion and GC-MS

Similar Documents

Determination of phenols and pharmaceuticals in municipal wastewaters from Polish treatment plants by ultrasound-assisted emulsification–microextraction followed by GC–MS

Monitoring pharmaceuticals and personal care products in reservoir water used for drinking water supply

Analytical method development for the determination of eight biocides in various environmental compartments and application for monitoring purposes

Detection of Benzo[a]pyrene in Fried Food by Ultrasound-Assisted Matrix Solid-Phase Dispersion and Isotope Dilution GC–MS

Temporal variation of heavy metal accumulation and translocation characteristics of narrow-leaved cattail (Typha angustifolia L.)

Prioritisation of organic contaminants in a river basin using chemical analyses and bioassays

A 3-year study on occurrence of emerging contaminants in an urban stream of São Paulo State of Southeast Brazil

New trends in the analytical determination of emerging contaminants and their transformation products in environmental waters

Presence of Pharmaceuticals and Hormones in Waters from Sewage Treatment Plants

Simultaneous determination of multiclass emerging contaminants in aquatic plants by ultrasound-assisted matrix solid-phase dispersion and GC-MS