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| Content Provider | Springer Nature Link |
|---|---|
| Author | Yuvakkumar, Rathinam Hong, Sun Ig |
| Copyright Year | 2015 |
| Abstract | The effect of incubation and aging on cassiterite type tetragonal rutile SnO$_{2}$ nanocrystals employing green synthesis technique has been investigated. The incubation and aging affected the compositional and morphological properties of SnO$_{2}$ and not influenced the structural properties of nanocrystals. The incubation and aging further influenced the particle shape and size of the obtained product. XRD results of the obtained product unambiguously revealed the cassiterite type tetragonal rutile phase of SnO$_{2}$ nanocrystals. The characteristic Raman peaks observed at 249, 476, 631 and 773 cm$^{−1}$ were respectively revealed infrared active (E$_{u}$), Raman active (E$_{g}$), (A$_{1g}$) and (B$_{2g}$) vibration modes of pure tetragonal rutile SnO$_{2}$ structure. 3d $_{3/2}$ and 3d $_{5/2}$ of XPS peaks observed at 496 and 487 eV was clearly revealed the Sn$^{4+}$ state in tetragonal rutile structure. The obtained TEM micrographs clearly revealed that the grain size and agglomeration was increased at higher incubation and aging treatments. |
| Starting Page | 2305 |
| Ending Page | 2310 |
| Page Count | 6 |
| File Format | |
| ISSN | 09574522 |
| Journal | Journal of Materials Science: Materials in Electronics |
| Volume Number | 26 |
| Issue Number | 4 |
| e-ISSN | 1573482X |
| Language | English |
| Publisher | Springer US |
| Publisher Date | 2015-01-23 |
| Publisher Place | Boston |
| Access Restriction | One Nation One Subscription (ONOS) |
| Subject Keyword | Optical and Electronic Materials Characterization and Evaluation of Materials |
| Content Type | Text |
| Resource Type | Article |
| Subject | Atomic and Molecular Physics, and Optics Biomaterials Biophysics Condensed Matter Physics Electronic, Optical and Magnetic Materials Bioengineering Electrical and Electronic Engineering Biomedical Engineering |
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