NDLI: Determination of volatile organic compounds including alcohols in refill fluids and cartridges of electronic cigarettes by headspace solid-phase micro extraction and gas chromatography

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Determination of volatile organic compounds including alcohols in refill fluids and cartridges of electronic cigarettes by headspace solid-phase micro extraction and gas chromatography–mass spectrometry

Content Provider	Springer Nature Link
Author	Lim, Hyun Hee Shin, Ho Sang
Copyright Year	2016
Abstract	An analytical method for the detection of 14 volatile organic compounds (VOCs) was developed to investigate VOCs in refill fluids and cartridges of electronic cigarettes (EC) using headspace solid-phase micro extraction (HS-SPME) coupled with gas chromatography–mass spectrometry (GC–MS). In total, 14 VOCs were identified and quantified in 283 flavored liquids, 21 nicotine liquids, and 12 disposable cartridges. The detected concentration ranges of the VOCs are as follows: benzene (0.008–2.28 mg L−1), toluene (0.006–0.687 mg L−1), ethylbenzene (0.01–1.21 mg L−1), m-xylene (0.002–1.13 mg L−1), p-xylene (0.007–2.8 mg L−1), o-xylene (0.004–2.27 mg L−1), styrene (0.011–0.339 mg L−1), ethyl acetate (0.3–669.9 mg L−1), ethanol (16–38,742 mg L−1), methanol (66–3375 mg L−1), pyridine (0.077–99.7 mg L−1), acetylpyrazine (0.077–147 mg L−1), 2,3,5-trimethylpyrazine (0.008–96.8 mg L−1), and octamethylcyclotetrasiloxane (0.1–57.2 mg L−1). Benzene, toluene, ethylbenzene, m-xylene, p-xylene, and o-xylene coexisted in samples, which may have originated from the use of petrogenic hydrocarbons as an extraction solvent for flavor and nicotine from natural plants. The maximum detected concentrations of benzene, methanol, and ethanol in liquid samples were found in quantities higher than their authorized maximum limits as residual solvents in pharmaceutical products.
Starting Page	1247
Ending Page	1256
Page Count	10
File Format	PDF
ISSN	16182642
Journal	Analytical and Bioanalytical Chemistry
Volume Number	409
Issue Number	5
e-ISSN	16182650
Language	English
Publisher	Springer Berlin Heidelberg
Publisher Date	2016-11-09
Publisher Place	Berlin, Heidelberg
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	Volatile organic compounds Electronic cigarette refill fluids Headspace solid-phase micro extraction Gas chromatography–mass spectrometry Analytical Chemistry Biochemistry Laboratory Medicine Characterization and Evaluation of Materials Food Science Monitoring/Environmental Analysis
Content Type	Text
Resource Type	Article
Subject	Analytical Chemistry Biochemistry

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