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| Content Provider | Royal Society of Chemistry (RSC) |
|---|---|
| Author | Wang, Bingrong Wang, Xiaohong Tu, Jinchun Cao, Yang Huang, Wei Chen, Yong Chen, Delun |
| Copyright Year | 2016 |
| Abstract | In this work, hollow Ni(OH)2 with low crystallinity was rapidly synthesized based on Cu2O template, which had a small particle size and high reaction activity. The resultant products were characterized by X-ray diffraction, field-emission scanning electron microscopy, transmission electron microscopy, X-ray photoelectron spectroscopy, Fourier transform infrared spectroscopy, and Raman spectroscopy. Results showed that Cu2O had a small particle size, and could shorten the reaction time for preparing hollow Ni(OH)2. Then, Ni(OH)2 was used to modify a glassy carbon electrode and found to perform well in ascorbic acid detection, with a linear range of 10 μM to 0.20 mM and the detection limit of 3 μM (S/N = 3). The sensitivity was 1747.71 μA mM−1 cm−2, which was due to the hollow Ni(OH)2 with low crystallinity. |
| Starting Page | 43598 |
| Ending Page | 43604 |
| Page Count | 7 |
| File Format | HTM / HTML PDF |
| ISSN | 20462069 |
| Volume Number | 6 |
| Issue Number | 49 |
| Journal | RSC Advances |
| DOI | 10.1039/c6ra05923f |
| Language | English |
| Publisher | Royal Society of Chemistry |
| Access Restriction | Open |
| Subject Keyword | Transmission electron microscopy Electrode Fourier Raman Photoemission spectroscopy Fourier-transform infrared spectroscopy Raman spectroscopy Scanning electron microscope Carbon X-ray photoelectron spectroscopy |
| Content Type | Text |
| Resource Type | Article |
| Subject | Chemistry Chemical Engineering |
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