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| Content Provider | Royal Society of Chemistry (RSC) |
|---|---|
| Author | Huvé, Marielle Mairesse, Gaëtan Nowogrocki, Guy Tendeloo, Gustaaf Van Vannier, Rose-Noëlle |
| Copyright Year | 1996 |
| Abstract | Bi4V2O11, the parent compound of the BIMEVOX family, has been studied by TEM and HREM, at room temperature and at high temperatures. Under the experimental conditions, Bi4V2O11 undergoes a VV–VIV reduction, ultimately leading to the formation of Bi6V3O16(Bi4V2O10.66) with VIV/VV= 1/2. This transformation is confirmed by in situ X-ray diffraction studies of Bi4V2O11 under reducing atmospheres up to 330 °C. The symmetry of the α-Bi4V2O11 polymorph, stable at ambient temperature, is dependent on the chemical purity of V2O5 used for the synthesis. |
| Starting Page | 1339 |
| Ending Page | 1345 |
| Page Count | 7 |
| File Format | |
| ISSN | 09599428 |
| Volume Number | 6 |
| Issue Number | 8 |
| Journal | Journal of Materials Chemistry |
| DOI | 10.1039/JM9960601339 |
| Language | English |
| Publisher | Royal Society of Chemistry |
| Access Restriction | Open |
| Subject Keyword | Transmission electron microscopy High-resolution transmission electron microscopy This Transformation X-ray crystallography Shapeshifting |
| Content Type | Text |
| Resource Type | Article |
| Subject | Chemistry Materials Chemistry |
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