NDLI: Solid-state synthesis of Nd-doped glass: thermal collapse of Nd<sup>3+</sup>-incorporated NaY zeolites

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Solid-state synthesis of Nd-doped glass: thermal collapse of Nd³⁺-incorporated NaY zeolites

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Inorganic Chemistry Frontiers Vol -3

Inorganic Chemistry Frontiers Vol -2

Inorganic Chemistry Frontiers Vol -1

Solid-state synthesis of Nd-doped glass: thermal collapse of Nd³⁺-incorporated NaY zeolites

Content Provider	Royal Society of Chemistry (RSC)
Author	Lin, Lin He, Dan-Nong Wang, Jing-Feng
Copyright Year	2017
Abstract	A solid-state synthesis of Nd-doped glass (NDG) in the acquisition aspect from the thermal collapse of Nd3+ ion-exchanged NaY zeolites has been conducted through experiments. The idea of rational design of the “perfect” NDG has been proven to be conceptually and practically feasible. The solid-synthesis method in comparison with the traditional molten-salt method has potential advantages of achieving “perfect” distribution, i.e., Nd3+ can be well-dispersed in the zeolite precursor and the final solid-state glass. The phase transformation from the Nd3+-exchanged zeolite NaY to Nd-doped glass was characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM) and differential scanning calorimetry (DSC), describing the migration and constraint of Nd3+ ions in the solid-state synthesis process. The fluorescence properties of the solid-state synthesized Nd-doped glass were also examined, and the results show that there is an optimized Nd3+ concentration associated with effective photoluminescence. The strategy of the solid-state process is possible to be applied to the synthesis of other functional glassy materials.
Starting Page	183
Ending Page	190
Page Count	8
File Format	HTM / HTML PDF
ISSN	20521553
Volume Number	4
Issue Number	1
Journal	Inorganic Chemistry Frontiers
DOI	10.1039/c6qi00428h
Language	English
Publisher	Royal Society of Chemistry
Access Restriction	Open
Subject Keyword	DSC Solid-state chemistry Zeolite X-ray crystallography Scanning electron microscope Differential scanning calorimetry Fluorescence Photoluminescence
Content Type	Text
Resource Type	Article
Subject	Inorganic Chemistry

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