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| Content Provider | World Health Organization (WHO)-Global Index Medicus |
|---|---|
| Author | Salem, Nahed M. H. Iskander, Magdi F. El Sayed, Laila Haase, Wolfgang |
| Description | Country affiliation: Egypt Author Affiliation: Salem NM ( Chemistry Department, Faculty of Science, Alexandria University, P.O. Box 426, Ibrahimia, Alexandria 21321, Egypt.); El Sayed L ( Chemistry Department, Faculty of Science, Alexandria University, P.O. Box 426, Ibrahimia, Alexandria 21321, Egypt.); Haase W ( Eduard-Zintl-Institute of Inorganic and Physical Chemistry, Darmstadt University of Technology, Petersenstrasse 20, 64287 Darmstadt, Germany.); Iskander MF ( Chemistry Department, Faculty of Science, Alexandria University, P.O. Box 426, Ibrahimia, Alexandria 21321, Egypt. Electronic address: m.iskander@link.net.) |
| Abstract | A series of diacetylmonoxime n-alkanoylhydrazones (H2L(n), n=4, 5, 6, 12 and 16) were prepared by the condensation of diacetylmonoxime with the corresponding n-alkanoylhydrazine in ethanol. The X-ray crystal structure of diacetylmonoxime octadecanoyl hydrazone has been solved and its molecular and supramolecular structures have been discussed. Both neutral dinuclear Cu(II) and Ni(II) complexes, [{M(L(n))}2] (M=Cu, Ni and n=4, 5, 6, 12 and 16) as well as cationic dinuclear Cu(II) complexes, [Cu2(L(n))(HL(n))]NO3 (n=12 and 16) have been also prepared and characterized by elemental analyses, FD- and ESI-mass spectra as well as IR, UV-Vis, (1)H NMR, (13)C NMR spectra. Variable temperature magnetic susceptibility measurements for dinuclear Cu(II) complexes have been also discussed. |
| ISSN | 13861425 |
| Volume Number | 134 |
| e-ISSN | 18733557 |
| Journal | Spectrochimica Acta Part A: Molecular and Biomolecular Spectroscopy |
| Language | English |
| Publisher | Elsevier |
| Publisher Date | 2015-01-05 |
| Publisher Place | Great Britain (UK) |
| Access Restriction | One Nation One Subscription (ONOS) |
| Subject Keyword | Coordination Complexes Chemistry Copper Nickel Chemistry Techniques, Synthetic Crystallography, X-ray Diacetyl Analogs & Derivatives Dimerization Magnetic Resonance Spectroscopy Magnetics Molecular Structure Spectrophotometry, Infrared Spectrophotometry, Ultraviolet Journal Article Discipline Spectroscopy |
| Content Type | Text |
| Resource Type | Article |
| Subject | Spectroscopy Atomic and Molecular Physics, and Optics Analytical Chemistry Instrumentation |
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