NDLI: ß-Estradiol and ethinyl-estradiol contamination in the rivers of the Carpathian Basin.

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ß-Estradiol and ethinyl-estradiol contamination in the rivers of the Carpathian Basin.

Content Provider	World Health Organization (WHO)-Global Index Medicus
Author	Avar, Péter G-Tóth, László Zrínyi, Zita Takátsy, Anikó Lovas, Sándor Maász, Gábor Pirger, Zsolt
Description	Country affiliation: Hungary Author Affiliation: Avar P ( Department of Analytical Biochemistry, Institute of Biochemistry and Medical Chemistry, University of Pécs, Pécs, 7624, Hungary. peter.avar@aok.pte.hu.); Zrínyi Z ( Adaptive Neuroethology, Department of Experimental Zoology, Tihany, 8237, Hungary.); Maász G ( Department of Analytical Biochemistry, Institute of Biochemistry and Medical Chemistry, University of Pécs, Pécs, 7624, Hungary.); Takátsy A ( Adaptive Neuroethology, Department of Experimental Zoology, Tihany, 8237, Hungary.); Lovas S ( Department of Analytical Biochemistry, Institute of Biochemistry and Medical Chemistry, University of Pécs, Pécs, 7624, Hungary.); G-Tóth L ( Adaptive Neuroethology, Department of Experimental Zoology, Tihany, 8237, Hungary.); Pirger Z ( Department of Hydrozoology, Balaton Limnological Institute, MTA Centre for Ecological Research, Tihany, 8237, Hungary.)
Abstract	17ß-Estradiol (E2) and 17 -ethinyl estradiol (EE2), which are environmental estrogens, have been determined with LC-MS in freshwater. Their sensitive analysis needs derivatization and therefore is very hard to achieve in multiresidue screening. We analyzed samples from all the large and some small rivers (River Danube, Drava, Mur, Sava, Tisza, and Zala) of the Carpathian Basin and from Lake Balaton. Freshwater was extracted on solid phase and derivatized using dansyl chloride. Separation was performed on a Kinetex XB-C18 column. Detection was achieved with a benchtop orbitrap mass spectrometer using targeted MS analysis for quantification. Limits of quantification were 0.05 ng/L (MS1) and 0.1 ng/L (MS/MS) for E2, and 0.001 ng/L (MS1) and 0.2 ng/L (MS/MS) for EE2. River samples contained n.d.-5.2 ng/L E2 and n.d.-0.68 ng/L EE2. Average levels of E2 and EE2 were 0.61 and 0.084 ng/L, respectively, in rivers, water courses, and Lake Balaton together, but not counting city canal water. EE2 was less abundant, but it was still present in almost all of the samples. In beach water samples from Lake Balaton, we measured 0.076-0.233 E2 and n.d.-0.133 EE2. A relative high amount of EE2 was found in river Zala (0.68 ng/L) and in Hévíz-Páhoki canal (0.52 ng/L), which are both in the catchment area of Lake Balaton (Hungary).
ISSN	09441344
Issue Number	12
Journal	Environmental Science and Pollution Research
Volume Number	23
e-ISSN	16147499
Language	English
Publisher	Springer
Publisher Date	2016-06-01
Publisher Place	Germany
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	Discipline Environmental Science Discipline Environmental Chemistry
Content Type	Text
Resource Type	Article
Subject	Environmental Chemistry Health, Toxicology and Mutagenesis Pollution Medicine

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