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| Content Provider | World Health Organization (WHO)-Global Index Medicus |
|---|---|
| Author | Prots, Yurii Baitinger, Michael Bobnar, Matej Wedel, Michael Burkhardt, Ulrich Grin, Yuri Böhme, Bodo Ormeci, Alim Liang, Ying Drathen, Christina Nguyen, Hong Duong |
| Description | Author Affiliation: Bobnar M ( Max-Planck-Institut für Chemische Physik fester Stoffe, Nöthnitzer Straße 40, 01187 Dresden, Germany. grin@cpfs.mpg.de.) |
| Abstract | The clathrate-I phase $Ba_{8}Al_{x}Si_{46−x}$ has been structurally characterized at the composition x = 6.9 (space group Pmn, no. 223, a = 10.4645(2) Å). A crystal structure model comprising the distribution of aluminium and silicon atoms in the clathrate framework was established: 5.7 Al atoms and 0.3 Si atoms occupy the crystallographic site 6c, while 1.2 Al atoms and 22.8 Si atoms occupy site 24k. The atomic distribution was established based on a combination of $^{27}Al$ and $^{29}Si$ NMR experiments, X-ray single-crystal diffraction and wavelength-dispersive X-ray spectroscopy. |
| ISSN | 14779226 |
| Issue Number | 28 |
| Journal | Dalton Trans. |
| Volume Number | 44 |
| e-ISSN | 13645447 |
| Language | English |
| Publisher | Royal Society of Chemistry |
| Publisher Date | 2015-07-28 |
| Publisher Place | Great Britain (UK) |
| Access Restriction | Subscribed |
| Subject Keyword | Chemistry |
| Content Type | Text |
| Resource Type | Article |
| Subject | Inorganic Chemistry |
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