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| Content Provider | World Health Organization (WHO)-Global Index Medicus |
|---|---|
| Author | Hintennach, Andreas Dinnebier, Robert E. Bender, Conrad L. Meiler, Markus Birkenmaier, Claudia Feinauer, Julian Schmidt, Volker Schleid, Thomas Krämer, Yvonne |
| Description | Author Affiliation: Krämer Y ( Deutsche ACCUmotive GmbH & Co. KG, Neue Straße 95, 73230 Kirchheim unter Teck (Germany), Fax: (+49) 711-3052-127780. yvonne.kraemer@daimler.com.) |
| Abstract | A novel approach for the marking of deposited lithium on graphite anodes from large automotive lithium-ion cells (≥6 Ah) is presented. Graphite anode samples were extracted from two different formats (cylindrical and pouch cells) of pristine and differently aged lithium-ion cells. The samples present a variety of anodes with various states of lithium deposition (also known as plating). A chemical modification was performed to metallic lithium deposited on the anode surface due to previous plating with isopropanol (IPA). After this procedure an oxygenated species was detected by scanning electron microscopy (SEM), which later was confirmed as $Li_{2}CO_{3}$ by Fourier transform infrared spectroscopy (FTIR) and X-ray powder diffraction (XRPD). A valuation of the covered area by $Li_{2}CO_{3}$ was carried out with an image analysis using energy-dispersive X-ray spectroscopy (EDX) and quantitative Rietveld refinement. |
| ISSN | 09476539 |
| e-ISSN | 15213765 |
| Journal | Chemistry - A European Journal |
| Issue Number | 16 |
| Volume Number | 21 |
| Language | English |
| Publisher | Wiley-VCH;ChemPubSoc Europe |
| Publisher Date | 2015-04-13 |
| Publisher Place | Germany |
| Access Restriction | Open |
| Subject Keyword | Chemistry |
| Content Type | Text |
| Resource Type | Article |
| Subject | Organic Chemistry Catalysis |
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