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| Content Provider | World Health Organization (WHO)-Global Index Medicus |
|---|---|
| Author | Reuter, Christian G. Romano, Rosana M. Mitzel, Norbert W. Canneva, Antonela Erben, Mauricio F. Della Védova, Carlos O. Vishnevskiy, Yury V. |
| Description | Author Affiliation: Canneva A ( Departamento de Química, Facultad de Ciencias Exactas, Universidad Nacional de La Plata, CC962, CEQUINOR (UNLP-CONICET, CCT, La Plata), La Plata (CP 1900) (República Argentina).); Erben MF ( Departamento de Química, Facultad de Ciencias Exactas, Universidad Nacional de La Plata, CC962, CEQUINOR (UNLP-CONICET, CCT, La Plata), La Plata (CP 1900) (República Argentina).); Romano RM ( Departamento de Química, Facultad de Ciencias Exactas, Universidad Nacional de La Plata, CC962, CEQUINOR (UNLP-CONICET, CCT, La Plata), La Plata (CP 1900) (República Argentina).); Vishnevskiy YV ( Universität Bielefeld, Lehrstuhl für Anorganische Chemie und Strukturchemie, Centrum für Molekulare Materialien CM2, Universitätsstrasse 25, 33615 Bielefeld (Germany).); Reuter CG ( Universität Bielefeld, Lehrstuhl für Anorganische Chemie und Strukturchemie, Centrum für Molekulare Materialien CM2, Universitätsstrasse 25, 33615 Bielefeld (Germany).); Mitzel NW ( Universität Bielefeld, Lehrstuhl für Anorganische Chemie und Strukturchemie, Centrum für Molekulare Materialien CM2, Universitätsstrasse 25, 33615 Bielefeld (Germany).); Della Védova CO ( Departamento de Química, Facultad de Ciencias Exactas, Universidad Nacional de La Plata, CC962, CEQUINOR (UNLP-CONICET, CCT, La Plata), La Plata (CP 1900) (República Argentina). carlosdv@quimica.unlp.edu.ar.) |
| Abstract | The gas-phase molecular structure of $(CH_{3})_{3}CSNO$ was investigated by using electron diffraction, allowing the first experimental geometrical parameters for an S-nitrosothiol species to be elucidated. Depending on the orientation of the SNO group, two conformers (anti and syn) are identified in the vapor of $(CH_{3})_{3}CSNO$ at room temperature, the syn conformer being less abundant. The conformational landscape is further scrutinized by using vibrational spectroscopy techniques, including gas-phase and matrix-isolation IR spectroscopy, resulting in a contribution of ca. 80:20 for the anti:syn abundance ratio, in good agreement with the computed value at the MP2(full)/cc-pVTZ level of approximation. The UV/Vis and resonance Raman spectra also show the occurrence of the conformational equilibrium in the liquid phase, with a moderate post-resonance Raman signature associated with the 350 nm electronic absorption. |
| ISSN | 09476539 |
| e-ISSN | 15213765 |
| Journal | Chemistry - A European Journal |
| Issue Number | 29 |
| Volume Number | 21 |
| Language | English |
| Publisher | Wiley-VCH;ChemPubSoc Europe |
| Publisher Date | 2015-07-13 |
| Publisher Place | Germany |
| Access Restriction | Open |
| Subject Keyword | Chemistry |
| Content Type | Text |
| Resource Type | Article |
| Subject | Organic Chemistry Catalysis |
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