NDLI: Identification of Carbonates as Additives in Pressure-Sensitive Adhesive Tape Substrate with Fourier Transform Infrared Spectroscopy (FTIR) and Its Application in Three Explosive Cases

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Identification of Carbonates as Additives in Pressure-Sensitive Adhesive Tape Substrate with Fourier Transform Infrared Spectroscopy (FTIR) and Its Application in Three Explosive Cases

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Year: 2013 Volume: 58 Issue: Supplementary 1

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Identification of Carbonates as Additives in Pressure-Sensitive Adhesive Tape Substrate with Fourier Transform Infrared Spectroscopy (FTIR) and Its Application in Three Explosive Cases

Content Provider	World Health Organization (WHO)-Global Index Medicus
Author	Lv, Jungang Feng, Jimin Zhang, Wen Shi, Rongguang Liu, Yong Wang, Zhaohong Zhao, Meng
Description	Country affiliation: China Author Affiliation: Lv J ( Procuratoral Technology and Information Research Center, Supreme People's Procuratorate, Beijing 100040, China. sdtaljg@163.com)
Abstract	Abstract: Pressure-sensitive tape is often used to bind explosive devices. It can become important trace evidence in many cases. Three types of calcium carbonate (heavy, light, and active $CaCO_{3}),$ which were widely used as additives in pressure-sensitive tape substrate, were analyzed with Fourier transform infrared spectroscopy (FTIR) in this study. A Spectrum GX 2000 system with a diamond anvil cell and a deuterated triglycine sulfate detector was employed for IR observation. Background was subtracted for every measurement, and triplicate tests were performed. Differences in positions of main peaks and the corresponding functional groups were investigated. Heavy $CaCO_{3}$ could be identified from the two absorptions near 873 and 855/cm, while light $CaCO_{3}$ only has one peak near 873/cm because of the low content of aragonite. Active $CaCO_{3}$ could be identified from the absorptions in the 2800–2900/cm region because of the existence of organic compounds. Tiny but indicative changes in the 878–853/cm region were found in the spectra of $CaCO_{3}$ with different content of aragonite and calcite. $CaCO_{3}$ in pressure-sensitive tape, which cannot be differentiated by scanning electron microscope/energy dispersive X-ray spectrometer and thermal analysis, can be easily identified using FTIR. The findings were successfully applied to three specific explosive cases and would be helpful in finding the possible source of explosive devices in future cases.
File Format	HTM / HTML
ISSN	00221198
Issue Number	1
Journal	Journal of Forensic Sciences
Volume Number	58
e-ISSN	15564029
Language	English
Publisher	Wiley-Blackwell
Publisher Date	2013-01-01
Publisher Place	United States
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	Discipline Forensic Sciences
Content Type	Text
Resource Type	Article
Subject	Genetics Pathology and Forensic Medicine

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Identification of Carbonates as Additives in Pressure-Sensitive Adhesive Tape Substrate with Fourier Transform Infrared Spectroscopy (FTIR) and Its Application in Three Explosive Cases