NDLI: Direct analyte-probed nanoextraction coupled to nanospray ionization-mass spectrometry of drug residues from latent fingerprints.

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Direct analyte-probed nanoextraction coupled to nanospray ionization-mass spectrometry of drug residues from latent fingerprints.

Content Provider	World Health Organization (WHO)-Global Index Medicus
Author	Clemons, Kristina Wiley, Rachel Waverka, Kristin Fox, James Dziekonski, Eric Verbeck, Guido F.
Description	Country affiliation: United States Author Affiliation: Clemons K ( Department of Chemistry, University of North Texas, 1155 Union Circle 305070, Denton, TX 76203, USA.)
Abstract	Here, we present a method of extracting drug residues from fingerprints via Direct Analyte-Probed Nanoextraction coupled to nanospray ionization-mass spectrometry (DAPNe-NSI-MS). This instrumental technique provides higher selectivity and lower detection limits over current methods, greatly reducing sample preparation, and does not compromise the integrity of latent fingerprints. This coupled to Raman microscopy is an advantageous supplement for location and identification of trace particles. DAPNe uses a nanomanipulator for extraction and differing microscopies for localization of chemicals of interest. A capillary tip with solvent of choice is placed in a nanopositioner. The surface to be analyzed is placed under a microscope, and a particle of interest is located. Using a pressure injector, the solvent is injected onto the surface where it dissolves the analyte, and then extracted back into the capillary tip. The solution is then directly analyzed via NSI-MS. Analyses of caffeine, cocaine, crystal methamphetamine, and ecstasy have been performed successfully.
File Format	HTM / HTML
ISSN	00221198
Issue Number	4
Volume Number	58
e-ISSN	15564029
Journal	Journal of Forensic Sciences
Language	English
Publisher	Wiley-Blackwell
Publisher Date	2013-07-01
Publisher Place	United States
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	Research Support, U.s. Gov't, Non-p.h.s. Dermatoglyphics Central Nervous System Stimulants Narcotics Humans Methamphetamine Sebum Discipline Forensic Sciences Journal Article Chemistry Microscopy Mass Spectrometry Analysis Spectrum Analysis, Raman Cocaine Sweat Nanotechnology Heroin N-methyl-3,4-methylenedioxyamphetamine Caffeine
Content Type	Text
Resource Type	Article
Subject	Genetics Pathology and Forensic Medicine

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Direct analyte-probed nanoextraction coupled to nanospray ionization-mass spectrometry of drug residues from latent fingerprints.

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