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Tin-containing silicates: alkali salts improve methyl lactate yield from sugars.

Content Provider	World Health Organization (WHO)-Global Index Medicus
Author	Tolborg, Søren Sádaba, Irantzu Osmundsen, Christian M. Fristrup, Peter Holm, Martin S. Taarning, Esben
Description	Author Affiliation: Tolborg S ( Haldor Topsøe A/S, New Business R&D, Nymøllevej 55, 2800, Kgs. Lyngby (Denmark))
Abstract	This study focuses on increasing the selectivity to methyl lactate from sugars using stannosilicates as heterogeneous catalyst. All groupâI ions are found to have a promoting effect on the resulting methyl lactate yield. Besides, the alkali ions can be added both during the preparation of the catalyst or directly to the solvent mixture to achieve the highest reported yield of methyl lactate (ca. 75 %) from sucrose at 170 °C in methanol. The beneficial effect of adding alkali to the reaction media applies not only to highly defect-free Sn-Beta prepared through the fluoride route, but also to materials prepared by post-treatment of dealuminated commercial Beta zeolites, as well as ordered mesoporous stannosilicates, in this case Sn-MCM-41 and Sn-SBA-15. These findings open the door to the possibility of using other preparation methods or different Sn-containing silicates with equally high methyl lactate yields as Sn-Beta.
File Format	HTM / HTML
ISSN	18645631
Issue Number	4
Volume Number	8
e-ISSN	1864564X
Journal	ChemSusChem
Language	English
Publisher	Wiley-VCH
Publisher Date	2015-02-01
Publisher Place	Germany
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	Lactates Research Support, Non-u.s. Gov't Chemistry Salts Sucrose Silicon Dioxide Discipline Sustainable Chemistry Tin Catalysis Zeolites Journal Article Metals, Alkali
Content Type	Text
Resource Type	Article
Subject	Energy Environmental Chemistry Materials Science Chemical Engineering

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