NDLI: Integrated multidimensional and comprehensive 2D GC analysis of fatty acid methyl esters.

Please wait, while we are loading the content...

Preliminary extraction of tannins by 1-butyl-3-methylimidazole bromide and its subsequent removal from Galla chinensis extract using macroporous resins.

Combining targeted and nontargeted data analysis for liquid chromatography/high-resolution mass spectrometric analyses.

Integrated multidimensional and comprehensive 2D GC analysis of fatty acid methyl esters.

Loading behavior of gatifloxacin in urine and lake water on a novel magnetic molecularly imprinted polymer used as extraction sorbent with spectrophotometric analysis

Determination of aromatic amines from textiles using dispersive liquid-liquid microextraction.

Pharmacokinetics of 2,3,5,4'-tetrahydroxystilbene-2-O-ß-D-glucoside in rat using ultra-performance LC-quadrupole TOF-MS.

Salting-out homogeneous liquid-liquid extraction in narrow-bore tube: extraction and preconcentration of phthalate esters from water.

Attempts to separate (-)- -thujone, (+)-ß-thujone epimers from camphor enantiomers by enantioselective HPLC with polarimetric detection.

Michrochip chromatography using an open-tubular microchannel and a ternary water-ACN-ethyl acetate mixture carrier solution.

Determination of three capsaicinoids in Capsicum annuum by pressurized liquid extraction combined with LC-MS/MS.

Sensitive monitoring of penicillin antibiotics in milk and honey treated by stir bar sorptive extraction based on monolith and LC-electrospray MS detection.

Organic-inorganic hybrid fluorous monolithic capillary column for selective solid-phase microextraction of perfluorinated persistent organic pollutants.

Prediction of extraction efficiency in supported liquid membrane with a stagnant acceptor phase by means of artificial neural network.

A comparison of various modes of liquid-liquid based microextraction techniques: determination of picric acid.

Low-density solvent-based vortex-assisted surfactant-enhanced emulsification liquid-liquid microextraction and its application.

Extraction of fullerenes from environmental matrices as affected by solvent characteristics and analyte concentration.

High-sensitive LC-MS/MS method for the simultaneous determination of mirodenafil and its major metabolite, SK-3541, in human plasma: application to microdose clinical trials of mirodenafil.

Influence of ionic liquids as electrolyte additives on chiral separation of dansylated amino acids by using Zn(II) complex mediated chiral ligand exchange CE.

Determination of crystal violet in seawater and seafood samples through off-line molecularly imprinted SPE followed by HPLC with diode-array detection.

Preparation and investigation of LC packing made by microwave-assisted solid-phase synthesis.

Analysis of volatile oil composition of Citrus aurantium L. by microwave-assisted extraction coupled to headspace solid-phase microextraction with nanoporous based fibers.

Simultaneous separation of jasmonic acid conjugates with amino acids by MEKC.

Year: 2013 Volume: 36 Issue: 4

Year: 2013 Volume: 36 Issue: 3

Year: 2013 Volume: 36 Issue: 2

Year: 2013 Volume: 36 Issue: 1

Year: 2013 Volume: 36 Issue: 9-10

Year: 2013 Volume: 36 Issue: 21-22

Year: 2012 Volume: 35

Year: 2011 Volume: 34

Year: 2010 Volume: 33

Year: 2009 Volume: 32

Year: 2008 Volume: 31

Year: 2007 Volume: 30

Year: 2005 Volume: 28

Integrated multidimensional and comprehensive 2D GC analysis of fatty acid methyl esters.

Content Provider	World Health Organization (WHO)-Global Index Medicus
Author	Zeng, Annie Xu Chin, Sung-Tong Marriott, Philip J.
Description	Country affiliation: Australia Author Affiliation: Zeng AX ( Centre for Green Chemistry, School of Chemistry, Monash University, Clayton, Victoria, Australia.)
Abstract	Fatty acid methyl ester (FAME) profiling in complex fish oil and milk fat samples was studied using integrated comprehensive 2D GC (GC × GC) and multidimensional GC (MDGC). Using GC × GC, FAME compounds--cis- and trans-isomers, and essential fatty acid isomers--ranging from C18 to C22 in fish oil and C18 in milk fat were clearly displayed in contour plot format according to structural properties and patterns, further identified based on authentic standards. Incompletely resolved regions were subjected to MDGC, with Cn (n = 18, 20) zones transferred to a (2)D column. Elution behavior of C18 FAME on various (2)D column phases (ionic liquids IL111, IL100, IL76, and modified PEG) was evaluated. Individual isolated Cn zones demonstrated about four-fold increased peak capacities. The IL100 provided superior separation, good peak shape, and utilization of elution space. For milk fat-derived FAME, the (2)D chromatogram revealed at least three peaks corresponding to C18:1, more than six peaks for cis/trans-C18:2 isomers, and two peaks for C18:3. More than 17 peaks were obtained for the C20 region of fish oil-derived FAMEs using MDGC, compared with ten peaks using GC × GC. The MDGC strategy is useful for improved FAME isomer separation and confirmation.
File Format	HTM / HTML
ISSN	16159306
Issue Number	5
Volume Number	36
e-ISSN	16159314
Journal	Journal of Separation Science
Language	English
Publisher	Wiley-VCH
Publisher Date	2013-03-01
Publisher Place	Germany
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	Discipline Analytical Discipline Chemistry Chromatography, Gas Methods Esters Analysis Fatty Acids Fish Oils Milk Chemistry Animals Cattle Evaluation Studies Journal Article
Content Type	Text
Resource Type	Article
Subject	Analytical Chemistry Filtration and Separation

Sl.	Authority	Responsibilities	Communication Details
1	Ministry of Education (GoI), Department of Higher Education	Sanctioning Authority	https://www.education.gov.in/ict-initiatives
2	Indian Institute of Technology Kharagpur	Host Institute of the Project: The host institute of the project is responsible for providing infrastructure support and hosting the project	https://www.iitkgp.ac.in
3	National Digital Library of India Office, Indian Institute of Technology Kharagpur	The administrative and infrastructural headquarters of the project	Dr. B. Sutradhar bsutra@ndl.gov.in
4	Project PI / Joint PI	Principal Investigator and Joint Principal Investigators of the project	Dr. B. Sutradhar bsutra@ndl.gov.in Prof. Saswat Chakrabarti will be added soon
5	Website/Portal (Helpdesk)	Queries regarding NDLI and its services	support@ndl.gov.in
6	Contents and Copyright Issues	Queries related to content curation and copyright issues	content@ndl.gov.in
7	National Digital Library of India Club (NDLI Club)	Queries related to NDLI Club formation, support, user awareness program, seminar/symposium, collaboration, social media, promotion, and outreach	clubsupport@ndl.gov.in
8	Digital Preservation Centre (DPC)	Assistance with digitizing and archiving copyright-free printed books	dpc@ndl.gov.in
9	IDR Setup or Support	Queries related to establishment and support of Institutional Digital Repository (IDR) and IDR workshops	idr@ndl.gov.in

Elucidation of fatty acid profiles in vegetable oils exploiting group-type patterning and enhanced sensitivity of comprehensive two-dimensional gas chromatography.

Gas chromatographic separation of fatty acid methyl esters on weakly polar capillary columns.

Preparation of fatty acid methyl esters for gas-liquid chromatography.

Acquisition of deeper knowledge on the human plasma fatty acid profile exploiting comprehensive 2-D GC.

Experimental designs for modeling retention patterns and separation efficiency in analysis of fatty acid methyl esters by gas chromatography-mass spectrometry.

Optimization of Fatty Acid Determination in Selected Fish and Microalgal Oils

A GC-magnetic sector MS method for identification and quantification of fatty acids in ewe milk by different acquisition modes.

Determination of Trace Levels of Fatty Acid Methyl Esters in Aviation Fuel by GC × GC–FID and Comparison with the Reference GC–MS Method

Quantification of trace fatty acid methyl esters in diesel fuel by using multidimensional gas chromatography with electron and chemical ionization mass spectrometry.

Integrated multidimensional and comprehensive 2D GC analysis of fatty acid methyl esters.

Similar Documents

Elucidation of fatty acid profiles in vegetable oils exploiting group-type patterning and enhanced sensitivity of comprehensive two-dimensional gas chromatography.

Gas chromatographic separation of fatty acid methyl esters on weakly polar capillary columns.

Preparation of fatty acid methyl esters for gas-liquid chromatography.

Acquisition of deeper knowledge on the human plasma fatty acid profile exploiting comprehensive 2-D GC.

Experimental designs for modeling retention patterns and separation efficiency in analysis of fatty acid methyl esters by gas chromatography-mass spectrometry.

Optimization of Fatty Acid Determination in Selected Fish and Microalgal Oils

A GC-magnetic sector MS method for identification and quantification of fatty acids in ewe milk by different acquisition modes.

Determination of Trace Levels of Fatty Acid Methyl Esters in Aviation Fuel by GC × GC–FID and Comparison with the Reference GC–MS Method

Quantification of trace fatty acid methyl esters in diesel fuel by using multidimensional gas chromatography with electron and chemical ionization mass spectrometry.

Integrated multidimensional and comprehensive 2D GC analysis of fatty acid methyl esters.