NDLI: Speciation analysis of orthophosphate and myo-inositol hexakisphosphate in soil- and plant-related samples by high-performance ion chromatography combined with inductively coupled plasma mass spectrometry

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Speciation analysis of orthophosphate and myo-inositol hexakisphosphate in soil- and plant-related samples by high-performance ion chromatography combined with inductively coupled plasma mass spectrometry

Content Provider	World Health Organization (WHO)-Global Index Medicus
Author	Rugova, Ariana Puschenreiter, Markus Santner, Jakob Fischer, Lisa Neubauer, Stefan Koellensperger, Gunda Hann, Stephan
Description	Country affiliation: Austria Author Affiliation: Rugova A ( Division of Analytical Chemistry, Department of Chemistry, University of Natural Resources and Life Sciences-BOKU, Vienna, Austria.)
Abstract	A novel method based on high-performance ion chromatography inductively coupled plasma mass spectrometry employing strong anion exchange chromatography with $HNO_{3}$ gradient elution for simultaneous analysis of orthophosphate and myo-inositol hexakisphosphate $(IP_{6})$ in soil solution and plant extracts is presented. As inductively coupled plasma mass spectrometry analysis of phosphorus at m/z 31 is hampered by N-based interferences, $^{31}P$ was measured as $^{31}P^{16}O^{+}$ at m/z 47 employing dynamic reaction cell technique with $O_{2}$ as reaction gas. Orthophosphate and $IP_{6}$ were separated within a total chromatographic run-time of 12 min revealing a limit of detection of 0.3 μmol/L. The coefficients of determination obtained in a working range of 1–100 and 1–30 μmol/L were 0.9991 for orthophosphate and 0.9968 for $IP_{6},$ respectively. The method was successfully applied to extracts from three different soils as well as root and shoot extracts of Brassica napus L. The precision of three independently prepared soil extracts was in the range of 4–10% relative standard deviation for $PO_{4}^{3−}$ and 3–8% relative standard deviation for $IP_{6}.$ Soil adsorption/desorption kinetics for $IP_{6}/orthophosphate$ were performed for investigating the sorption behavior of the two P species in the experimental soils.
File Format	HTM / HTML
ISSN	16159306
Issue Number	14
Volume Number	37
e-ISSN	16159314
Journal	Journal of Separation Science
Language	English
Publisher	Wiley-VCH
Publisher Date	2014-07-01
Publisher Place	Germany
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	Discipline Analytical Discipline Chemistry Brassica Napus Chemistry Chromatography, High Pressure Liquid Methods Inositol Analogs & Derivatives Mass Spectrometry Phosphates Plant Extracts Plants Soil Isolation & Purification Molecular Structure Plant Roots Plant Shoots Evaluation Studies Journal Article Research Support, Non-u.s. Gov't
Content Type	Text
Resource Type	Article
Subject	Analytical Chemistry Filtration and Separation

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Speciation analysis of orthophosphate and myo-inositol hexakisphosphate in soil- and plant-related samples by high-performance ion chromatography combined with inductively coupled plasma mass spectrometry

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