NDLI: Green Chemistry Approach: Synthesis, Characterization and Antimicrobial Activity of Hydrazones and Their Metal Complexes

Content Provider	Springer Nature Link
Author	Singh, Shivani Akhtar, Rubeena Sharma, Neelam Kumar, Devendra
Copyright Year	2012
Abstract	Six new metal complexes of Co(II), Ni(II) and Cu(II) derived from bis-(furfuryl) succinic acid dihydrazone and bis-(2-acetyl thiophene) succinic acid dihydrazone have been synthesized by adopting green chemistry approach, i.e. microwave assisted method. By microwave assisted synthesis, a considerable increase in the reaction rate has been observed and that too, with better yields. Synthesized compounds have been characterized by running their TLC for single spot, repeated melting point determinations, elemental analyses, IR, $^{1}$H-NMR, electronic spectral studies and magnetic susceptibility measurements. The elemental analyses, spectral data and magnetic susceptibility results revealed their metal:ligand (1:1) ratio with coordination number 6. The ligand and metal complexes showed good activity against Staphylococcus aureus, Pseudomonas aeruginosa and fungi Aspergillus niger and Candida albicans.
Starting Page	295
Ending Page	301
Page Count	7
File Format	PDF
ISSN	03698203
Journal	Proceedings of the National Academy of Sciences, India Section A: Physical Sciences
Volume Number	82
Issue Number	4
e-ISSN	22501762
Language	English
Publisher	Springer-Verlag
Publisher Date	2012-07-08
Publisher Place	India
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	NMR Antimicrobial activity Applied and Technical Physics IR Atomic, Molecular, Optical and Plasma Physics Electronic Quantum Physics Microwave assisted synthesis Physics
Content Type	Text
Resource Type	Article
Subject	Physics and Astronomy Biochemistry, Genetics and Molecular Biology

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