NDLI: Preparation of a solid-state ion-selective electrode based on polypyrrole conducting polymer for magnesium ion

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Preparation of a solid-state ion-selective electrode based on polypyrrole conducting polymer for magnesium ion

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Journal of the Iranian Chemical Society : Volume 11, Issue 1, February 2014

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Preparation of a solid-state ion-selective electrode based on polypyrrole conducting polymer for magnesium ion

Content Provider	Springer Nature Link
Author	Arvand, Majid Mosayebzadeh, Zahra Ansari, Reza
Copyright Year	2013
Abstract	In this study, a potentiometric sensor based on a pencil graphite electrode (PGE) coated with polypyrrole doped with Titan yellow dye (PPy/TY) was prepared for potentiometric determination of magnesium ion in aqueous solutions. The structural characteristics of magnesium sensor electrode (PGE/PPy/TYMg) were studied using scanning electron microscopy and Fourier transform infrared along with energy-dispersive spectroscopy. Under the optimal conditions, the electrode reveals a good Nernstian behavior with slope of 28.27 ± 0.40 mV per decade over the concentration range of 1.0 × 10$^{−5}$–5.0 × 10$^{−2}$ M and a detection limit of 6.28 × 10$^{−6}$ M. The potentiometric response of fabricated electrode toward magnesium ion was found to be independent of the pH of the test solution in the pH range of 4.5–8.0. The electrode showed fast response time (<10 s) and good shelf lifetime (>2 months). The prepared magnesium sensor electrode can also be used as an indicator electrode in potentiometric titration of Mg$^{2+}$ with EDTA with distinguished end point. The electrode revealed good selectivity with respect to many cations including alkali, alkaline earth, transition and heavy metal ions. The introduced magnesium electrode was used for measurement of Mg$^{2+}$ ion in real samples without any serious interferences from other ions.
Starting Page	447
Ending Page	456
Page Count	10
File Format	PDF
ISSN	1735207X
Journal	Journal of the Iranian Chemical Society
Volume Number	11
Issue Number	2
e-ISSN	17352428
Language	English
Publisher	Springer Berlin Heidelberg
Publisher Date	2013-08-04
Publisher Place	Berlin, Heidelberg
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	Analytical Chemistry Magnesium electrode Physical Chemistry Titan yellow Biochemistry Inorganic Chemistry Potentiometry Polypyrrole Organic Chemistry
Content Type	Text
Resource Type	Article
Subject	Chemistry

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