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| Content Provider | Springer Nature Link |
|---|---|
| Author | Rizzetti, Tiele M. Souza, Maiara P. Prestes, Osmar D. Adaime, Martha B. Zanella, Renato |
| Copyright Year | 2016 |
| Abstract | A simple and rapid sample preparation method was developed and validated for multi-class analysis of veterinary drug residues in bovine kidney and liver. Sample preparation procedure was performed using acetonitrile and trichloroacetic acid for protein precipitation followed by ultra-high-performance liquid chromatography tandem mass spectrometry (UHPLC-MS/MS) analysis. The proposed method was validated according to the criteria of the Commission Decision 2002/657/EC evaluating linearity, selectivity, accuracy and precision, determination limit (CCα), and detection capacity (CCβ). Linearity presented r $^{2}$ ≥ 0.99 for all the target compounds, and recoveries ranged from 80 to 110 % with RSD ≤17 % for intra- and inter-day assay. Values of CCα and CCβ ranged from 11 to 1096 and from 12 to 1191 μg kg$^{−1}$, respectively. The proposed sample preparation followed by UHPLC-MS/MS analysis was suitable for the determination of 20 veterinary drug residues in bovine kidney and liver in routine analysis. Method applicability was evaluated using commercial samples. |
| Starting Page | 854 |
| Ending Page | 864 |
| Page Count | 11 |
| File Format | |
| ISSN | 19369751 |
| Journal | Food Analytical Methods |
| Volume Number | 10 |
| Issue Number | 4 |
| e-ISSN | 1936976X |
| Language | English |
| Publisher | Springer US |
| Publisher Date | 2016-09-05 |
| Publisher Place | New York |
| Access Restriction | One Nation One Subscription (ONOS) |
| Subject Keyword | Multi-class Veterinary drugs Kidney Liver UHPLC-MS/MS Food Science Chemistry/Food Science Microbiology Analytical Chemistry |
| Content Type | Text |
| Resource Type | Article |
| Subject | Analytical Chemistry Safety Research Safety, Risk, Reliability and Quality Applied Microbiology and Biotechnology Food Science |
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