NDLI: Synthesis and characterization of a thermo-sensitive poly(N-methyl acryloylglycine methyl ester) used as a drug release carrier

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Synthesis and characterization of a thermo-sensitive poly(N-methyl acryloylglycine methyl ester) used as a drug release carrier

Content Provider	Springer Nature Link
Author	Deng, Kui Lin Zhong, Hai Bin Jiao, Yi Suo Fan, Ting Qiao, Xiao Zhang, Peng Fei Ren, Xiao Bo
Copyright Year	2010
Abstract	In this article, poly(N-methyl acryloylglycine methyl ester) (PNMAME) was prepared as a novel thermosensitive material with a lower critical solution temperature (LCST) at around 49.5°C. The chemical structures of the monomer NMAME and PNMAME were characterized by $^{1}$H NMR and IR measurements. The LCST was investigated systematically as a function of PNMAME concentration, inorganic salt solution and pH value. The results indicated that LCST of PNMAME was obviously dependent on PNMAME concentration and pH. The LCST was increased with a decrease in pH value and PNMAME concentration. To obtain a thermo-sensitive hydrogel with the phase transition temperature close to human body temperature, the copolymerization was conducted between NMAME and N-acryloylglycine ethyl ester (NAGEE). The release behavior of caffeine was evaluated at different temperatures and contents of cross-linkers (N, N-methylenebis(acrylamide) (NMBA)). The increase of cross-linker content led to a decrease in the release rate of caffeine due to higher crossing density in the hydrogel network. In addition, a faster release of caffeine from the hydrogel with 3% NMBA at 37°C was found in contrast to that at 18°C.
Starting Page	164
Ending Page	170
Page Count	7
File Format	PDF
ISSN	16737377
Journal	Frontiers of Materials Science in China
Volume Number	4
Issue Number	2
e-ISSN	16737482
Language	English
Publisher	SP Higher Education Press
Publisher Date	2010-04-29
Publisher Institution	Chinese Universities
Publisher Place	Heidelberg
Access Restriction	Subscribed
Subject Keyword	thermo-sensitive N-methyl acryloylglycine methyl ester (NMAME) lower critical solution temperature (LCST) drug release Materials Science
Content Type	Text
Resource Type	Article
Subject	Materials Science

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