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Recycling process of spent battery modules in used hybrid electric vehicles using physical/chemical treatments

Content Provider	Springer Nature Link
Author	Kim, Sookyung Yang, Donghyo Rhee, Kangin Sohn, Jeongsoo
Copyright Year	2014
Abstract	The physical treatment/chemical treatments for recycling of spent lithium-ion battery modules in used hybrid electric vehicles as cathodic active materials were performed. The result by physical treatment showed that over 95 % valuable metals such as Co, Li, Ni, and Mn were concentrated in 65-mesh during a grinding time 2 min, while just 2.7 % Al was concentrated from spent lithium-ion batteries which were completely electric discharged after 70 min. Through reductive leaching with H$_{2}$O$_{2}$ and H$_{2}$SO$_{4}$, leaching efficiency of valuable metals with 65-mesh powder was almost 99 % Co, Mn, Ni, and Li under the conditions of 2 M H$_{2}$SO$_{4}$, 5 vol% H$_{2}$O$_{2}$, 60 °C, 300 rpm, 50 g/500 mL, and 2 h. After removing some impurities such as Cu, Al, and Fe, the leaching solutions containing Co, Mn, Ni, and Li could be utilized for manufacturing the precursor of cathodic active material of Li-ion battery. The precursor was manufactured by co-precipitation from the filtrate after calibration of Co, Mn, and Ni concentration adding NaOH and NH$_{4}$OH under the conditions over pH 11, 30 °C, 150 rpm, and 24 h. To maintain the pH, 11 is most important level for making homogeneous spherical Co–Mn–Ni hydroxide.
Starting Page	2447
Ending Page	2456
Page Count	10
File Format	PDF
ISSN	09226168
Journal	Research on Chemical Intermediates
Volume Number	40
Issue Number	7
e-ISSN	15685675
Language	English
Publisher	Springer Netherlands
Publisher Date	2014-05-28
Publisher Place	Dordrecht
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	Recycling Spent lithium battery module Hybrid electric vehicles Co-precipitation Co–Mn–Ni hydroxide Catalysis Physical Chemistry Inorganic Chemistry
Content Type	Text
Resource Type	Article
Subject	Chemistry

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