NDLI: Nanostructured ZnO hexagons and optical properties

Content Provider	Springer Nature Link
Author	Thorat, J. H. Kanade, K. G. Nikam, L. K. Chaudhari, P. D. Kale, B. B.
Copyright Year	2010
Abstract	We report the solvothermal synthesis of nanostructured ZnO hexagons by hydrothermal method via intermediate zinc adipate. The intermediate zinc adipate was obtained using precursors zinc acetate and adipic acid in aqueous and organic medium. Detailed XRD analysis of the zinc adipate was studied for the first time. Thermal study of intermediate showed the formation of ZnO at 400 °C. XRD study demonstrated the existence of wrutzite ZnO of high degree of crystallinity with crystallite size in the range of 20–25 nm. Scanning Electron Microscopy (SEM) showed distinguished morphology in different medium. Transmission Electron Microscopy (TEM) demonstrated nanostructured ZnO hexagons with average size 25–50 nm. The band gap for aqueous and organic mediated ZnO was found to be 3.24 and 3.26 eV, respectively. The band gap obtained is higher than the bulk ZnO, which implies nanocrystalline nature of the material.
Starting Page	394
Ending Page	399
Page Count	6
File Format	PDF
ISSN	09574522
Journal	Journal of Materials Science: Materials in Electronics
Volume Number	22
Issue Number	4
e-ISSN	1573482X
Language	English
Publisher	Springer US
Publisher Date	2010-06-27
Publisher Place	Boston
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	Characterization and Evaluation of Materials Optical and Electronic Materials
Content Type	Text
Resource Type	Article
Subject	Atomic and Molecular Physics, and Optics Biomaterials Biophysics Condensed Matter Physics Electronic, Optical and Magnetic Materials Bioengineering Electrical and Electronic Engineering Biomedical Engineering

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