NDLI: Reduction and characterizations of iron particles: influence of reduction parameters

Content Provider	Springer Nature Link
Author	Karaagac, Oznur Kockar, Hakan Ebin, Burcak Gurmen, Sebahattin
Copyright Year	2013
Abstract	Iron particles have some applications as electromagnetic devices in magnetic recording and data storage technology due to their small sizes and high data storage capacity. The devices can be advanced by improving the properties of existing materials according to the production parameters. Thus, the influences of reduction parameters on the properties of iron particles were studied. The iron particles were reduced from superparamagnetic iron oxide nanoparticles by altering reduction parameters under hydrogen atmosphere at high (400 °C) temperature. The structural analysis of the films was carried out using the X-ray diffraction (XRD) and high resolution transmission electron microscopy (HRTEM) techniques. The XRD data revealed that the crystal textures changed for the particles reduced at each parameter. And, the crystal structure turns from the cubic spinel structure of magnetite and body centered cubic (bcc) structure of iron to the bcc iron as the reduction time increases from 15 to 240 min. Then, the similar structure change can be seen for the samples reduced at increasing hydrogen flow rates. The HRTEM studies revealed that the surface morphology of the films strongly depend on the flow rate. Finally, magnetite peaks weaken and then disappear as the precursor mass decreases to the lowest value. The average crystallite sizes were found to be consistent with changing crystal structure. Furthermore, the magnetic characteristics studied by a vibrating sample magnetometer were observed to be affected by the parameters. Besides, magnetic differences may arise from the variation of crystal structure and crystal sizes caused by individual reduction parameters of reduction time, hydrogen flow rate and precursor mass.
Starting Page	2602
Ending Page	2609
Page Count	8
File Format	PDF
ISSN	09574522
Journal	Journal of Materials Science: Materials in Electronics
Volume Number	24
Issue Number	7
e-ISSN	1573482X
Language	English
Publisher	Springer US
Publisher Date	2013-02-28
Publisher Place	Boston
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	Optical and Electronic Materials Characterization and Evaluation of Materials
Content Type	Text
Resource Type	Article
Subject	Atomic and Molecular Physics, and Optics Biomaterials Biophysics Condensed Matter Physics Electronic, Optical and Magnetic Materials Bioengineering Electrical and Electronic Engineering Biomedical Engineering

Sl.	Authority	Responsibilities	Communication Details
1	Ministry of Education (GoI), Department of Higher Education	Sanctioning Authority	https://www.education.gov.in/ict-initiatives
2	Indian Institute of Technology Kharagpur	Host Institute of the Project: The host institute of the project is responsible for providing infrastructure support and hosting the project	https://www.iitkgp.ac.in
3	National Digital Library of India Office, Indian Institute of Technology Kharagpur	The administrative and infrastructural headquarters of the project	Dr. B. Sutradhar bsutra@ndl.gov.in
4	Project PI / Joint PI	Principal Investigator and Joint Principal Investigators of the project	Dr. B. Sutradhar bsutra@ndl.gov.in Prof. Saswat Chakrabarti will be added soon
5	Website/Portal (Helpdesk)	Queries regarding NDLI and its services	support@ndl.gov.in
6	Contents and Copyright Issues	Queries related to content curation and copyright issues	content@ndl.gov.in
7	National Digital Library of India Club (NDLI Club)	Queries related to NDLI Club formation, support, user awareness program, seminar/symposium, collaboration, social media, promotion, and outreach	clubsupport@ndl.gov.in
8	Digital Preservation Centre (DPC)	Assistance with digitizing and archiving copyright-free printed books	dpc@ndl.gov.in
9	IDR Setup or Support	Queries related to establishment and support of Institutional Digital Repository (IDR) and IDR workshops	idr@ndl.gov.in

Characterizations of Electrodeposited NiCoFe Ternary Alloys: Influence of deposition potential

Preparation and characterization of iron phthalocyanine polymer magnetic materials

Characterization of electrosynthesized iron diselenide thin films

Solvothermal preparation of iron nanosheets

Influence of tungsten particles on the electrical properties of AlN ceramic

Characterization of CVD tungsten deposited by silane reduction

Preparation and characterizations of tungsten oxide electrochromic nanomaterials

Growth and various characterizations of LiHSO$_{4}$ single crystals

Influence of HVP trimming on primary parameters of thick resistive films

Reduction and characterizations of iron particles: influence of reduction parameters

Similar Documents

Characterizations of Electrodeposited NiCoFe Ternary Alloys: Influence of deposition potential

Preparation and characterization of iron phthalocyanine polymer magnetic materials

Characterization of electrosynthesized iron diselenide thin films

Solvothermal preparation of iron nanosheets

Influence of tungsten particles on the electrical properties of AlN ceramic

Characterization of CVD tungsten deposited by silane reduction

Preparation and characterizations of tungsten oxide electrochromic nanomaterials

Growth and various characterizations of LiHSO$_{4}$ single crystals

Influence of HVP trimming on primary parameters of thick resistive films

Reduction and characterizations of iron particles: influence of reduction parameters