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| Content Provider | Springer Nature Link |
|---|---|
| Author | Venugopal, Meenu Saravana Kumar, S. Nissamudeen, K. M. Padma Kumar, H. |
| Copyright Year | 2016 |
| Abstract | Nanocrystalline Ceria (CeO$_{2}$) was synthesized through auto-ignited combustion technique. The X-ray diffraction studies of CeO$_{2}$ nanoparticles have shown that the as-prepared powder was single phase, crystalline and has a face centred cubic structure. The phase purity of the powder was further examined using Fourier Transform Infrared and Raman spectroscopic techniques. The transmission electron microscopic studies have shown that the particle size of the as prepared powder was in the range of 30–40 nm. The band gap of nanoparticles as calculated from the absorption spectrum was found to be 3.51 eV. The photoluminescent spectrum of the samples exhibited a number of emission peaks which forms a broad band emission between 400 and 500 nm originating from $^{2}$T$_{2g}$(5d)–$^{2}$F$_{7/2}$, $^{2}$F$_{5/2}$(4f) transition of Ce$^{3+}$ ion due to spin–orbit coupling under the influence of O $_{h}$ crystal field. The nanopowders were sintered to about 95 % of the theoretical density at 1450 °C for 2 h. The microstructure of the sintered surface was examined using scanning electron microscopy. The dielectric constant (ε$_{r}$) and loss tangent (tanδ) at 5 MHz are found to be about 25.1 and 0.0118 respectively. The complex impedance plots show semicircular arcs resolving at high temperature which confirms the existence of the non-Debye type of relaxation in the sintered CeO$_{2}$ samples. |
| Starting Page | 9496 |
| Ending Page | 9502 |
| Page Count | 7 |
| File Format | |
| ISSN | 09574522 |
| Journal | Journal of Materials Science: Materials in Electronics |
| Volume Number | 27 |
| Issue Number | 9 |
| e-ISSN | 1573482X |
| Language | English |
| Publisher | Springer US |
| Publisher Date | 2016-05-24 |
| Publisher Place | New York |
| Access Restriction | One Nation One Subscription (ONOS) |
| Subject Keyword | Optical and Electronic Materials Characterization and Evaluation of Materials |
| Content Type | Text |
| Resource Type | Article |
| Subject | Atomic and Molecular Physics, and Optics Biomaterials Biophysics Condensed Matter Physics Electronic, Optical and Magnetic Materials Bioengineering Electrical and Electronic Engineering Biomedical Engineering |
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