NDLI: Synthesis of Pb(Zr, Ti)O$_{3}$ Nanopowders by Milling Coprecipitation Method

Content Provider	Springer Nature Link
Author	Kim, Myong Ho Golovchanski, A. Lee, Soon Il Park, Tae Gone Song, Tae Kwon
Copyright Year	2004
Abstract	Nano-size powders of lead zirconate titanate (PZT) were fabricated by a new milling coprecipitation method (MCP) improved from the conventional wet ball milling and precipitation. This method consists of slurry preparation from nanoparticles of TiO$_{2}$ with aqueous solution of ZrO(NO$_{3}$)$_{2}$ and Pb(NO$_{3}$)$_{2}$ with zirconia ball mill media, followed by precipitation with NH$_{4}$OH as precipitant. Milling media (1mm and 3mm balls) improves the precipitation homogeneity during processing. Single-phase perovskite structure of PZT was formed at a calcination temperature of 500$^{∘}$C and powders of 50 nm particle size were obtained. Powders were characterized using TG-DTA, SEM and XRD methods. Sintering ability of powders and piezoelectric properties of the ceramics were also investigated.
Starting Page	367
Ending Page	371
Page Count	5
File Format	PDF
ISSN	13853449
Journal	Journal of Electroceramics
Volume Number	13
Issue Number	1-3
e-ISSN	15738663
Language	English
Publisher	Kluwer Academic Publishers
Publisher Date	2004-01-01
Publisher Place	Boston
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	PZT piezoelectric nano-size coprecipitation mechano-chemistry Polymer Sciences Optical and Electronic Materials Characterization and Evaluation Materials Ceramics, Glass, Composites, Natural Methods Crystallography
Content Type	Text
Resource Type	Article
Subject	Ceramics and Composites Materials Chemistry Mechanics of Materials Condensed Matter Physics Electronic, Optical and Magnetic Materials Electrical and Electronic Engineering

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