NDLI: Fast and simple procedure for fractionation of zinc in soil using an ultrasound probe and FAAS detection. Validation of the analytical method and evaluation of the uncertainty budget

Content Provider	Springer Nature Link
Author	Leśniewska, Barbara Kisielewska, Katarzyna Wiater, Józefa Godlewska Żyłkiewicz, Beata
Copyright Year	2015
Abstract	A new fast method for determination of mobile zinc fractions in soil is proposed in this work. The three-stage modified BCR procedure used for fractionation of zinc in soil was accelerated by using ultrasounds. The working parameters of an ultrasound probe, a power and a time of sonication, were optimized in order to acquire the content of analyte in soil extracts obtained by ultrasound-assisted sequential extraction (USE) consistent with that obtained by conventional modified Community Bureau of Reference (BCR) procedure. The content of zinc in extracts was determined by flame atomic absorption spectrometry. The developed USE procedure allowed for shortening the total extraction time from 48 h to 27 min in comparison to conventional modified BCR procedure. The method was fully validated, and the uncertainty budget was evaluated. The trueness and reproducibility of the developed method was confirmed by analysis of certified reference material of lake sediment BCR-701. The applicability of the procedure for fast, low costs and reliable determination of mobile zinc fraction in soil, which may be useful for assessing of anthropogenic impacts on natural resources and environmental monitoring purposes, was proved by analysis of different types of soil collected from Podlaskie Province (Poland).
Starting Page	1
Ending Page	13
Page Count	13
File Format	PDF
ISSN	01676369
Journal	Environmental Monitoring and Assessment
Volume Number	188
Issue Number	1
e-ISSN	15732959
Language	English
Publisher	Springer International Publishing
Publisher Date	2015-12-14
Publisher Place	Cham
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	Sequential extraction Modified BCR procedure Zinc fractions Ultrasound probe Uncertainty budged Environmental Monitoring/Analysis Environmental Management Ecotoxicology Atmospheric Protection/Air Quality Control/Air Pollution Ecology
Content Type	Text
Resource Type	Article
Subject	Pollution Medicine Management, Monitoring, Policy and Law

Sl.	Authority	Responsibilities	Communication Details
1	Ministry of Education (GoI), Department of Higher Education	Sanctioning Authority	https://www.education.gov.in/ict-initiatives
2	Indian Institute of Technology Kharagpur	Host Institute of the Project: The host institute of the project is responsible for providing infrastructure support and hosting the project	https://www.iitkgp.ac.in
3	National Digital Library of India Office, Indian Institute of Technology Kharagpur	The administrative and infrastructural headquarters of the project	Dr. B. Sutradhar bsutra@ndl.gov.in
4	Project PI / Joint PI	Principal Investigator and Joint Principal Investigators of the project	Dr. B. Sutradhar bsutra@ndl.gov.in Prof. Saswat Chakrabarti will be added soon
5	Website/Portal (Helpdesk)	Queries regarding NDLI and its services	support@ndl.gov.in
6	Contents and Copyright Issues	Queries related to content curation and copyright issues	content@ndl.gov.in
7	National Digital Library of India Club (NDLI Club)	Queries related to NDLI Club formation, support, user awareness program, seminar/symposium, collaboration, social media, promotion, and outreach	clubsupport@ndl.gov.in
8	Digital Preservation Centre (DPC)	Assistance with digitizing and archiving copyright-free printed books	dpc@ndl.gov.in
9	IDR Setup or Support	Queries related to establishment and support of Institutional Digital Repository (IDR) and IDR workshops	idr@ndl.gov.in

Fast and simple procedure for fractionation of zinc in soil using an ultrasound probe and FAAS detection. Validation of the analytical method and evaluation of the uncertainty budget

An ultrasound-assisted procedure for fast screening of mobile fractions of Cd, Pb and Ni in soil. Insight into method optimization and validation

An ultrasound-assisted procedure for fast screening of mobile fractions of Cd, Pb and Ni in soil. Insight into method optimization and validation

Fast and simple procedure for fractionation of zinc in soil using an ultrasound probe and FAAS detection. Validation of the analytical method and evaluation of the uncertainty budget

Comparison of unmodified and modified BCR sequential extraction schemes for the fractionation of heavy metals in shrimp aquaculture sludge from Selangor, Malaysia

Determination of heavy metals in lower Sakarya river sediments using a BCR-sequential extraction procedure

Zinc speciation in sediments from a polluted river, as an estimate of its bioaccesibility

Investigation of trace elements in agricultural soils by BCR sequential extraction method and its transfer to wheat plants

Fractions and leaching characteristics of mercury in coal

Fast and simple procedure for fractionation of zinc in soil using an ultrasound probe and FAAS detection. Validation of the analytical method and evaluation of the uncertainty budget

Similar Documents

Fast and simple procedure for fractionation of zinc in soil using an ultrasound probe and FAAS detection. Validation of the analytical method and evaluation of the uncertainty budget

An ultrasound-assisted procedure for fast screening of mobile fractions of Cd, Pb and Ni in soil. Insight into method optimization and validation

An ultrasound-assisted procedure for fast screening of mobile fractions of Cd, Pb and Ni in soil. Insight into method optimization and validation

Fast and simple procedure for fractionation of zinc in soil using an ultrasound probe and FAAS detection. Validation of the analytical method and evaluation of the uncertainty budget

Comparison of unmodified and modified BCR sequential extraction schemes for the fractionation of heavy metals in shrimp aquaculture sludge from Selangor, Malaysia

Determination of heavy metals in lower Sakarya river sediments using a BCR-sequential extraction procedure

Zinc speciation in sediments from a polluted river, as an estimate of its bioaccesibility

Investigation of trace elements in agricultural soils by BCR sequential extraction method and its transfer to wheat plants

Fractions and leaching characteristics of mercury in coal

Fast and simple procedure for fractionation of zinc in soil using an ultrasound probe and FAAS detection. Validation of the analytical method and evaluation of the uncertainty budget