NDLI: LC Analysis of Aliphatic Primary Amines and Diamines After Derivatization with 2,6-Dimethyl-4-quinolinecarboxylic Acid N-Hydroxysuccinimide Ester

Content Provider	Springer Nature Link
Author	Huang, Ke Jing Wei, Cai Yun Xie, Wan Zhen Liu, Yan Ming Chen, Yong Hong Zhang, Jun Feng
Copyright Year	2009
Abstract	A method for sensitive simultaneous analysis of aliphatic primary amines and diamines has been developed and validated. The compounds were analyzed by reversed-phase high-performance liquid chromatography after pre-column derivatization with 2,6-dimethyl-4-quinolinecarboxylic acid N-hydroxysuccinimide ester as fluorescent probe. The derivatization reaction was performed at 50 °C for 40 min in 0.1 mol L−1 borax buffer solution (pH 7.5). The resulting fluorophores were separated to baseline on a C18 column and fluorimetrically detected at λ ex/λ em = 326/409 nm. Detection limits were in the range 0.50–0.02 nmol L−1. The method was successfully used for analysis of aliphatic amines in water, human urine, and serum.
Starting Page	747
Ending Page	752
Page Count	6
File Format	PDF
ISSN	00095893
Journal	Chromatographia
Volume Number	70
Issue Number	5-6
e-ISSN	16121112
Language	English
Publisher	Vieweg Verlag
Publisher Date	2009-07-28
Publisher Place	Wiesbaden
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	Column liquid chromatography Fluorescence detection Aliphatic primary amines and diamines 2,6-Dimethyl-4-quinolinecarboxylic acid N-hydroxysuccinimide ester Measurement Science and Instrumentation Plant Sciences Biochemistry Pharmacy Organic Chemistry Analytical Chemistry
Content Type	Text
Resource Type	Article
Subject	Organic Chemistry Analytical Chemistry Biochemistry Clinical Biochemistry

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