NDLI: Headspace solid phase microextraction of volatile aromatic hydrocarbons using a steel wire coated with an electrochemically prepared nanocomposite consisting of polypyrrole, carbon nanotubes, and titanium oxide

Content Provider	Springer Nature Link
Author	Sarafraz Yazdi, Ali Rounaghi, Gholamhossein Vatani, Hossein Razavipanah, Iman Amiri, Amirhassan
Copyright Year	2014
Abstract	We have prepared a new material for solid-phase microextraction (SPME) of volatile aromatic hydrocarbons by electropolymerization of pyrrole, carbon nanotubes, and titanium oxide on the surface of a stainless steel wire. This fiber-like wire was used for the headspace solid-phase microextraction of mixtures of benzene, toluene, ethylbenzene, and o-xylene (BTEX), followed by their quantitation by GC with FID detection. The fiber is easily prepared, robust, thermally stable, and has good extraction efficiency. Under optimal conditions, the detection limits (at an SNR of 3) are in the range from 0.01 to 0.04 ng mL−1, and the limits of quantification (at an SNR of 10) are between 0.03 and 0.09 ng mL−1. The relative standard deviations (RSDs) for one fiber (i. e. the repeatability; for n = 5) range from 3.5 to 5.6 %, while the RSDs between fibers or from batch to batch (i.e. the reproducibility; for n = 3) are in the range from 5.9 to 8.1 %. The method was successfully applied to (spiked) real water samples, the relative recovery percentages being between 93.7 and 106.2 %. Graphical abstract In the present work, polypyrrole-carbon nanotubes–titanium oxide composite coated onto 438 stainless steel wire have been successfully synthesized and were applied as adsorbent for the 439 headspace solid-phase microextraction of benzene, toluene, ethylbenzene, and o-xylene (BTEX).
Starting Page	217
Ending Page	225
Page Count	9
File Format	PDF
ISSN	00263672
Journal	Microchimica Acta
Volume Number	182
Issue Number	1-2
e-ISSN	14365073
Language	English
Publisher	Springer Vienna
Publisher Date	2014-07-09
Publisher Place	Vienna
Access Restriction	One Nation One Subscription (ONOS)
Subject Keyword	Solid-phase microextraction Carbon nanotubes Titanium oxide nanoparticles Polypyrrole BTEX Nanochemistry Nanotechnology Characterization and Evaluation of Materials Analytical Chemistry Microengineering
Content Type	Text
Resource Type	Article
Subject	Analytical Chemistry

Sl.	Authority	Responsibilities	Communication Details
1	Ministry of Education (GoI), Department of Higher Education	Sanctioning Authority	https://www.education.gov.in/ict-initiatives
2	Indian Institute of Technology Kharagpur	Host Institute of the Project: The host institute of the project is responsible for providing infrastructure support and hosting the project	https://www.iitkgp.ac.in
3	National Digital Library of India Office, Indian Institute of Technology Kharagpur	The administrative and infrastructural headquarters of the project	Dr. B. Sutradhar bsutra@ndl.gov.in
4	Project PI / Joint PI	Principal Investigator and Joint Principal Investigators of the project	Dr. B. Sutradhar bsutra@ndl.gov.in Prof. Saswat Chakrabarti will be added soon
5	Website/Portal (Helpdesk)	Queries regarding NDLI and its services	support@ndl.gov.in
6	Contents and Copyright Issues	Queries related to content curation and copyright issues	content@ndl.gov.in
7	National Digital Library of India Club (NDLI Club)	Queries related to NDLI Club formation, support, user awareness program, seminar/symposium, collaboration, social media, promotion, and outreach	clubsupport@ndl.gov.in
8	Digital Preservation Centre (DPC)	Assistance with digitizing and archiving copyright-free printed books	dpc@ndl.gov.in
9	IDR Setup or Support	Queries related to establishment and support of Institutional Digital Repository (IDR) and IDR workshops	idr@ndl.gov.in

Electrochemical fabrication of polypyrrole/hazelnut shells modified carbon nanocomposite sorbent for determination of polycyclic aromatic hydrocarbons using headspace solid-phase microextraction-gas chromatography

Nanostructured polypyrrole for automated and electrochemically controlled in-tube solid-phase microextraction of cationic nitrogen compounds

Solid phase headspace microextraction of tricyclic antidepressants using a directly prepared nanocomposite consisting of graphene, CTAB and polyaniline

Fibers coated with a graphene-polyaniline nanocomposite for the headspace solid-phase microextraction of organochlorine pesticides from seawater samples

HP-SPME of Volatile Polycyclic Aromatic Hydrocarbons from Water Using Multiwalled Carbon Nanotubes Coated on a Steel Fiber through Electrophoretic Deposition

Headspace solid phase microextraction of nicotine using thin layer chromatography plates modified with carbon dots

Electrochemical In Situ Fabrication of Titanium Dioxide Nanotubes on a Titanium Wire as a Fiber Coating for Solid-Phase Microextraction of Polycyclic Aromatic Hydrocarbons

Metal organic framework MIL-101 coated fiber for headspace solid phase microextraction of volatile aromatic compounds

Application of Polypyrrole Coated Stainless-Steel Wire to the Headspace Solid-Phase Microextraction of Aliphatic Amines

Headspace solid phase microextraction of volatile aromatic hydrocarbons using a steel wire coated with an electrochemically prepared nanocomposite consisting of polypyrrole, carbon nanotubes, and titanium oxide

Similar Documents

Electrochemical fabrication of polypyrrole/hazelnut shells modified carbon nanocomposite sorbent for determination of polycyclic aromatic hydrocarbons using headspace solid-phase microextraction-gas chromatography

Nanostructured polypyrrole for automated and electrochemically controlled in-tube solid-phase microextraction of cationic nitrogen compounds

Solid phase headspace microextraction of tricyclic antidepressants using a directly prepared nanocomposite consisting of graphene, CTAB and polyaniline

Fibers coated with a graphene-polyaniline nanocomposite for the headspace solid-phase microextraction of organochlorine pesticides from seawater samples

HP-SPME of Volatile Polycyclic Aromatic Hydrocarbons from Water Using Multiwalled Carbon Nanotubes Coated on a Steel Fiber through Electrophoretic Deposition

Headspace solid phase microextraction of nicotine using thin layer chromatography plates modified with carbon dots

Electrochemical In Situ Fabrication of Titanium Dioxide Nanotubes on a Titanium Wire as a Fiber Coating for Solid-Phase Microextraction of Polycyclic Aromatic Hydrocarbons

Metal organic framework MIL-101 coated fiber for headspace solid phase microextraction of volatile aromatic compounds

Application of Polypyrrole Coated Stainless-Steel Wire to the Headspace Solid-Phase Microextraction of Aliphatic Amines

Headspace solid phase microextraction of volatile aromatic hydrocarbons using a steel wire coated with an electrochemically prepared nanocomposite consisting of polypyrrole, carbon nanotubes, and titanium oxide