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Phosphine-catalyzed [3 + 2] cycloaddition of phthalazinium dicyanomethanides with allenoates: highly efficient synthesis of 1,2,3,10b-tetrahydropyrrolo[2,1-a]phthalazine derivatives
| Content Provider | Semantic Scholar |
|---|---|
| Author | Yuan, Chunhao Zhou, Leijie Sun, Zhanhu Guo, Hongchao |
| Copyright Year | 2016 |
| Abstract | The phosphine-catalyzed [3 + 2] cycloaddition between phthalazinium dicyanomethanides and allenoates, has been achieved in dichloromethane at room temperature, providing a broad range of novel heterocyclic compounds, 1,2,3,10b-tetrahydropyrrolo[2,1-a]phthalazine derivatives, as single (Z)-isomers in excellent yields (88–99% yield). All reactions are operationally simple and proceed very fast under mild reaction conditions. |
| Starting Page | 77931 |
| Ending Page | 77936 |
| Page Count | 6 |
| File Format | PDF HTM / HTML |
| DOI | 10.1039/C6RA13643E |
| Volume Number | 6 |
| Alternate Webpage(s) | http://www.rsc.org/suppdata/c6/ra/c6ra13643e/c6ra13643e1.pdf |
| Alternate Webpage(s) | https://doi.org/10.1039/C6RA13643E |
| Language | English |
| Access Restriction | Open |
| Content Type | Text |
| Resource Type | Article |